1-(3,4-dimethoxyphenyl)-2-oxiranylethanol

Base Information

Chemical Name:1-(3,4-dimethoxyphenyl)-2-oxiranylethanol
CAS No.:880262-17-9
Molecular Formula:C₁₂H₁₆O₄
Molecular Weight:224.257
Hs Code.:

Synonyms:1-(3,4-dimethoxyphenyl)-2-oxiranylethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3,4-dimethoxyphenyl)-2-oxiranylethanol

Chemical Property:

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Technology Process of 1-(3,4-dimethoxyphenyl)-2-oxiranylethanol

There total 1 articles about 1-(3,4-dimethoxyphenyl)-2-oxiranylethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 97387-80-9,5452-46-0
1-(3,4-dimethoxy-phenyl)-but-3-en-1-ol

: 880262-17-9
1-(3,4-dimethoxyphenyl)-2-oxiranylethanol

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 20 ℃; for 60h;
DOI:10.1002/ejoc.200500424

Reference yield: 80.0%

: 880262-17-9
1-(3,4-dimethoxyphenyl)-2-oxiranylethanol

: 106-96-7
propargyl bromide

: 880262-22-6
2-[2-(3,4-dimethoxyphenyl)-2-(prop-2-ynyloxy)ethyl]oxirane

Guidance literature:: With sodium hydride; In tetrahydrofuran; dimethyl sulfoxide; at 0 - 20 ℃; for 8.5h;
DOI:10.1002/ejoc.200500424

Reference yield:

: 880262-17-9
1-(3,4-dimethoxyphenyl)-2-oxiranylethanol

: rac-[(2S,4R)-2-(3,4-dimethoxyphenyl)-5-methylenetetrahydro-2H-pyran-4-yl]methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaH / tetrahydrofuran; dimethylsulfoxide / 8.5 h / 0 - 20 °C

2: titanocene dichloride; zinc / tetrahydrofuran / 2.17 h / 20 °C

With titanocene dichloride; sodium hydride; zinc; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1002/ejoc.200500424