2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name: 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside
CAS No.:133157-05-8
Molecular Formula:C₃₂H₃₇NO₁₂
Molecular Weight:627.645
Hs Code.:

<methyl N-(diphenylmethylene)-L-threoninate-3-yl> 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Synonyms: 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

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Technology Process of 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

There total 3 articles about 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 572-09-8,3068-32-4,4026-32-8,6919-96-6,13242-53-0,14227-54-4,14795-18-7,19186-59-5,19285-38-2,21698-13-5,29907-26-4,53369-42-9,60619-58-1,61303-35-3,67337-79-5,69127-37-3,70749-15-4,72002-90-5,75247-30-2,75880-74-9,78418-57-2,102339-89-9,102339-90-2,103530-40-1,114028-03-4,114718-45-5,138514-70-2,138514-71-3
2,3,4,6-tetra-O-acetyl-D-glucopyranosyl bromide

: 130740-27-1
N-diphenylmethylene-L-threonine methyl ester

: 133157-05-8
2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4039(00)74833-7

Reference yield: 17.0%

: 130740-27-1
N-diphenylmethylene-L-threonine methyl ester

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 133157-05-8
2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: 1,2-O-<<oxy>ethylidene-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; for 14h; Ambient temperature;
DOI:10.1021/ja00052a022

Reference yield:

: 1013-88-3
Benzophenone imine

: 133157-05-8
2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / CH₂Cl₂ / 24 h / Ambient temperature

2: 64 percent / 4A molecular sieves, AgOTf / CH₂Cl₂ / 14 h / Ambient temperature

With 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1021/ja00052a022