(R)-1-ethyl hydrogen 3-benzyloxycarbonylamino-3-ethoxycarbonylsuccinate

Base Information

Chemical Name:(R)-1-ethyl hydrogen 3-benzyloxycarbonylamino-3-ethoxycarbonylsuccinate
CAS No.:1239129-15-7
Molecular Formula:C₁₇H₂₁NO₈
Molecular Weight:367.356
Hs Code.:

Synonyms:(R)-1-ethyl hydrogen 3-benzyloxycarbonylamino-3-ethoxycarbonylsuccinate

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Chemical Property of (R)-1-ethyl hydrogen 3-benzyloxycarbonylamino-3-ethoxycarbonylsuccinate

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Technology Process of (R)-1-ethyl hydrogen 3-benzyloxycarbonylamino-3-ethoxycarbonylsuccinate

There total 2 articles about (R)-1-ethyl hydrogen 3-benzyloxycarbonylamino-3-ethoxycarbonylsuccinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1239129-13-5
diethyl 2-benzyloxycarbonylamino-2-ethoxycarbonylsuccinate

: 1239129-15-7
(R)-1-ethyl hydrogen 3-benzyloxycarbonylamino-3-ethoxycarbonylsuccinate

Guidance literature:: With ethanol; In aq. phosphate buffer; at 30 ℃; for 20h; pH=6.5; Concentration; Reagent/catalyst; Time; Enzymatic reaction;

Reference yield:

: 3005-66-1
diethyl 2-benzyloxycarbonylaminomalonate

: 1239129-15-7
(R)-1-ethyl hydrogen 3-benzyloxycarbonylamino-3-ethoxycarbonylsuccinate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 1 h / 50 °C

2: ethanol / aq. phosphate buffer / 20 h / 30 °C / pH 6.5 / Enzymatic reaction

With ethanol; potassium carbonate; potassium iodide; In aq. phosphate buffer; N,N-dimethyl-formamide;

Reference yield: 84.0%

: 1239129-15-7
(R)-1-ethyl hydrogen 3-benzyloxycarbonylamino-3-ethoxycarbonylsuccinate

: 1239129-17-9
(R)-diethyl 2-benzyloxycarbonylamino-2-carbamoylsuccinate

Guidance literature:: (R)-1-ethyl hydrogen 3-benzyloxycarbonylamino-3-ethoxycarbonylsuccinate; With triethylamine; isobutyl chloroformate; In tetrahydrofuran; at -15 ℃; for 0.0833333h;

With ammonium hydroxide; In tetrahydrofuran; at -15 ℃; for 1h;