benzyl (E)-(2'S,3'S)-2,3-O-[2',3'-dimethoxybutane-2',3'-diyl]-4-C-nitromethylene-β-D-erythro-pentapyranoside

Base Information

Chemical Name:benzyl (E)-(2'S,3'S)-2,3-O-[2',3'-dimethoxybutane-2',3'-diyl]-4-C-nitromethylene-β-D-erythro-pentapyranoside
CAS No.:1309358-04-0
Molecular Formula:C₁₉H₂₅NO₈
Molecular Weight:395.409
Hs Code.:

Synonyms:benzyl (E)-(2'S,3'S)-2,3-O-[2',3'-dimethoxybutane-2',3'-diyl]-4-C-nitromethylene-β-D-erythro-pentapyranoside

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Chemical Property of benzyl (E)-(2'S,3'S)-2,3-O-[2',3'-dimethoxybutane-2',3'-diyl]-4-C-nitromethylene-β-D-erythro-pentapyranoside

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Technology Process of benzyl (E)-(2'S,3'S)-2,3-O-[2',3'-dimethoxybutane-2',3'-diyl]-4-C-nitromethylene-β-D-erythro-pentapyranoside

There total 3 articles about benzyl (E)-(2'S,3'S)-2,3-O-[2',3'-dimethoxybutane-2',3'-diyl]-4-C-nitromethylene-β-D-erythro-pentapyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₉NO₁₀

: 1309358-04-0
benzyl (E)-(2'S,3'S)-2,3-O-[2',3'-dimethoxybutane-2',3'-diyl]-4-C-nitromethylene-β-D-erythro-pentapyranoside

Guidance literature:: With silica gel; In dichloromethane; at 50 ℃; for 24h;
DOI:10.1021/ol200942g

Reference yield:

: C₂₁H₂₉NO₁₀

: 1309358-04-0
benzyl (E)-(2'S,3'S)-2,3-O-[2',3'-dimethoxybutane-2',3'-diyl]-4-C-nitromethylene-β-D-erythro-pentapyranoside

: 1309358-09-5
benzyl (2'S,3'S)-4-deoxy-2,3-O-[2',3'-dimethoxybutane-2',3'-diyl]-4-C-nitromethyl-β-D-arabinopyranoside

: 1309358-10-8
benzyl (2'S,3'S)-4-deoxy-2,3-O-[2',3'-dimethoxybutane-2',3'-diyl]-4-C-nitromethyl-α-L-xylopyranoside

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 - 20 ℃;
DOI:10.1021/ol200942g

Reference yield:

: benzyl(2'S,3'S)-2,3-O-[2',3'-dimethoxybutane-2',3'-diyl]-4-C-nitromethyl-α-L-xylopyranoside

: 1309358-04-0
benzyl (E)-(2'S,3'S)-2,3-O-[2',3'-dimethoxybutane-2',3'-diyl]-4-C-nitromethylene-β-D-erythro-pentapyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / 7 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate / ethanol / 0 - 20 °C

With sodium tetrahydroborate; toluene-4-sulfonic acid; In ethanol;
DOI:10.1021/ol200942g