C₂₆H₃₈O₂Si

Base Information

Chemical Name:C₂₆H₃₈O₂Si
CAS No.:1404304-70-6
Molecular Formula:C₂₆H₃₈O₂Si
Molecular Weight:410.672
Hs Code.:

C<sub>26</sub>H<sub>38</sub>O<sub>2</sub>Si

Synonyms:C₂₆H₃₈O₂Si

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Chemical Property of C₂₆H₃₈O₂Si

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Technology Process of C₂₆H₃₈O₂Si

There total 4 articles about C₂₆H₃₈O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1404304-64-8
C₂₃H₃₂O₂Si

: 1730-25-2
allylmagnesium bromide

: 1404304-70-6
C₂₆H₃₈O₂Si

Guidance literature:: With copper(l) iodide; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol302409g

Reference yield:

: 33467-76-4
(E)-hept-2-en-1-ol

: 1404304-70-6
C₂₆H₃₈O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1: triphenylphosphine; tetrachloromethane / 24 h / 80 °C / Inert atmosphere

2: (DHQD)_2PHAL; methanesulfonamide; potassium osmate(VI) dihydrate; potassium hexacyanoferrate(III); potassium carbonate; sodium hydrogencarbonate / tert-butyl alcohol; water / 4 h / 0 °C / Inert atmosphere

3: sodium hydroxide / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

4: 1H-imidazole / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere

5: copper(l) iodide / tetrahydrofuran; diethyl ether / 1 h / -78 - 20 °C / Inert atmosphere

With (DHQD)_2PHAL; 1H-imidazole; tetrachloromethane; potassium osmate(VI) dihydrate; copper(l) iodide; methanesulfonamide; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine; sodium hydroxide; potassium hexacyanoferrate(III); In tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol; 2: |Sharpless Dihydroxylation;
DOI:10.1021/ol302409g

Reference yield:

: 68703-33-3
(E)-1-chloro-2-heptene

: 1404304-70-6
C₂₆H₃₈O₂Si

Guidance literature:: Multi-step reaction with 4 steps

1: (DHQD)_2PHAL; methanesulfonamide; potassium osmate(VI) dihydrate; potassium hexacyanoferrate(III); potassium carbonate; sodium hydrogencarbonate / tert-butyl alcohol; water / 4 h / 0 °C / Inert atmosphere

2: sodium hydroxide / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

3: 1H-imidazole / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere

4: copper(l) iodide / tetrahydrofuran; diethyl ether / 1 h / -78 - 20 °C / Inert atmosphere

With (DHQD)_2PHAL; 1H-imidazole; potassium osmate(VI) dihydrate; copper(l) iodide; methanesulfonamide; sodium hydrogencarbonate; potassium carbonate; sodium hydroxide; potassium hexacyanoferrate(III); In tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol; 1: |Sharpless Dihydroxylation;
DOI:10.1021/ol302409g