N^ω-trityl-L-glutaminyl-L-tryptophanyl-L-aspartyl (β-benzyl ester)-L-phenylalanyl-glycine benzyl ester

Base Information

• Chemical Name: N^ω-trityl-L-glutaminyl-L-tryptophanyl-L-aspartyl (β-benzyl ester)-L-phenylalanyl-glycine benzyl ester
• CAS No.: 848693-01-6
• Molecular Formula: C₆₄H₆₃N₇O₉
• Molecular Weight: 1074.25

Synonyms:N^ω-trityl-L-glutaminyl-L-tryptophanyl-L-aspartyl (β-benzyl ester)-L-phenylalanyl-glycine benzyl ester

Chemical Property of N^ω-trityl-L-glutaminyl-L-tryptophanyl-L-aspartyl (β-benzyl ester)-L-phenylalanyl-glycine benzyl ester

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Technology Process of N^ω-trityl-L-glutaminyl-L-tryptophanyl-L-aspartyl (β-benzyl ester)-L-phenylalanyl-glycine benzyl ester

There total 1 articles about N^ω-trityl-L-glutaminyl-L-tryptophanyl-L-aspartyl (β-benzyl ester)-L-phenylalanyl-glycine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

Fmoc-Gln(Trt)-Trp-Asp(Bn)-Phe-Gly-OBn → Nω-trityl-L-glutaminyl-L-tryptophanyl-L-aspartyl (β-benzyl ester)-L-phenylalanyl-glycine benzyl ester (848693-01-6)

Guidance literature:

With piperidine; In N,N-dimethyl-formamide;

DOI:10.1248/cpb.52.1479

Reference yield: 95.0%

{4-[3-(4-benzyloxy-phenyl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionylamino]-phenoxy}-acetic acid (848693-00-5) + Nω-trityl-L-glutaminyl-L-tryptophanyl-L-aspartyl (β-benzyl ester)-L-phenylalanyl-glycine benzyl ester (848693-01-6) → C103H95N9O15

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1248/cpb.52.1479

Reference yield: 81.0%

{3-[3-(4-benzyloxy-phenyl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionylamino]-phenoxy}-acetic acid (848692-99-9) + Nω-trityl-L-glutaminyl-L-tryptophanyl-L-aspartyl (β-benzyl ester)-L-phenylalanyl-glycine benzyl ester (848693-01-6) → C103H95N9O15

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1248/cpb.52.1479

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