1-(4-chloro-phenyl)-2-(2,4-dichloro-phenyl)-5-methanesulfonyl-1H-imidazole-4-carboxylic acid piperidin-1-ylamide

Base Information

Chemical Name:1-(4-chloro-phenyl)-2-(2,4-dichloro-phenyl)-5-methanesulfonyl-1H-imidazole-4-carboxylic acid piperidin-1-ylamide
CAS No.:847474-88-8
Molecular Formula:C₂₂H₂₁Cl₃N₄O₃S
Molecular Weight:527.859
Hs Code.:

Synonyms:1-(4-chloro-phenyl)-2-(2,4-dichloro-phenyl)-5-methanesulfonyl-1H-imidazole-4-carboxylic acid piperidin-1-ylamide

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Chemical Property of 1-(4-chloro-phenyl)-2-(2,4-dichloro-phenyl)-5-methanesulfonyl-1H-imidazole-4-carboxylic acid piperidin-1-ylamide

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Technology Process of 1-(4-chloro-phenyl)-2-(2,4-dichloro-phenyl)-5-methanesulfonyl-1H-imidazole-4-carboxylic acid piperidin-1-ylamide

There total 2 articles about 1-(4-chloro-phenyl)-2-(2,4-dichloro-phenyl)-5-methanesulfonyl-1H-imidazole-4-carboxylic acid piperidin-1-ylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: N,N-diisopropylethylamine (Hunig's base)

: 847474-86-6
1-(4-chlorophenyl)-2-(2,4-dichlorophenyl)-5-methylsulfonyl-1H-imidazole-4-carboxylic acid

: O-benzotriazol-1-yl-N,N, N',N'-tetramethyluronium hexafluorophosphate (HBTU)

: 2213-43-6
1-Aminopiperidine

: 847474-88-8
1-(4-chloro-phenyl)-2-(2,4-dichloro-phenyl)-5-methanesulfonyl-1H-imidazole-4-carboxylic acid piperidin-1-ylamide

Guidance literature:: In ethyl acetate; acetonitrile;

Reference yield: 84.0%

: 847474-86-6
1-(4-chlorophenyl)-2-(2,4-dichlorophenyl)-5-methylsulfonyl-1H-imidazole-4-carboxylic acid

: 2213-43-6
1-Aminopiperidine

: 847474-88-8
1-(4-chloro-phenyl)-2-(2,4-dichloro-phenyl)-5-methanesulfonyl-1H-imidazole-4-carboxylic acid piperidin-1-ylamide

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃;
DOI:10.1016/j.bmcl.2010.03.068