C₂₃H₃₂N₂O₄S

Base Information

Chemical Name:C₂₃H₃₂N₂O₄S
CAS No.:877659-87-5
Molecular Formula:C₂₃H₃₂N₂O₄S
Molecular Weight:432.584
Hs Code.:

C<sub>23</sub>H<sub>32</sub>N<sub>2</sub>O<sub>4</sub>S

Synonyms:C₂₃H₃₂N₂O₄S

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Chemical Property of C₂₃H₃₂N₂O₄S

Chemical Property:

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Technology Process of C₂₃H₃₂N₂O₄S

There total 10 articles about C₂₃H₃₂N₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 877659-54-6
1,6-dimethyl-cyclohex-3-enecarbaldehyde

: 877659-87-5
C₂₃H₃₂N₂O₄S

Guidance literature:: Multi-step reaction with 9 steps

1.1: Jones' reagent / acetone / 1 h / 0 °C

2.1: aq. NaHCO₃; KI; I₂ / tetrahydrofuran / 6 h / 0 °C

3.1: DBU / tetrahydrofuran / 12 h / Heating

4.1: methanol / 3 h / 20 °C

5.1: pyridinium chlorochromate / CH₂Cl₂ / 1 h / 20 °C

6.1: lithium di-tert-butyl-biphenylide / tetrahydrofuran / 0.17 h / -78 °C

6.2: CuCN / tetrahydrofuran / 1 h / -78 °C

6.3: Me₃SiCl / tetrahydrofuran / 1 h / -78 °C

7.1: O₃ / CH₂Cl₂ / 0.33 h / -78 °C

7.2: dimethyl sulfide / -78 - 20 °C

8.1: p-TSA / benzene / 14 h / Heating

9.1: aq. HCl / ethanol / 1.5 h / Heating

With hydrogenchloride; jones' reagent; lithium di-tert-butyl-biphenylide; iodine; sodium hydrogencarbonate; toluene-4-sulfonic acid; ozone; 1,8-diazabicyclo[5.4.0]undec-7-ene; pyridinium chlorochromate; potassium iodide; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetone; benzene;
DOI:10.1021/ja057483x

Reference yield:

: 421555-41-1
5-hydroxy-1,2-dimethyl-cyclohex-3-enecarboxylic acid lactone

: 877659-87-5
C₂₃H₃₂N₂O₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: methanol / 3 h / 20 °C

2.1: pyridinium chlorochromate / CH₂Cl₂ / 1 h / 20 °C

3.1: lithium di-tert-butyl-biphenylide / tetrahydrofuran / 0.17 h / -78 °C

3.2: CuCN / tetrahydrofuran / 1 h / -78 °C

3.3: Me₃SiCl / tetrahydrofuran / 1 h / -78 °C

4.1: O₃ / CH₂Cl₂ / 0.33 h / -78 °C

4.2: dimethyl sulfide / -78 - 20 °C

5.1: p-TSA / benzene / 14 h / Heating

6.1: aq. HCl / ethanol / 1.5 h / Heating

With hydrogenchloride; lithium di-tert-butyl-biphenylide; toluene-4-sulfonic acid; ozone; pyridinium chlorochromate; In tetrahydrofuran; methanol; ethanol; dichloromethane; benzene;
DOI:10.1021/ja057483x

Reference yield:

: 877659-55-7
1,2-dimethyl-5-oxo-cyclohex-3-enecarboxylic acid methyl ester

: 877659-87-5
C₂₃H₃₂N₂O₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium di-tert-butyl-biphenylide / tetrahydrofuran / 0.17 h / -78 °C

1.2: CuCN / tetrahydrofuran / 1 h / -78 °C

1.3: Me₃SiCl / tetrahydrofuran / 1 h / -78 °C

2.1: O₃ / CH₂Cl₂ / 0.33 h / -78 °C

2.2: dimethyl sulfide / -78 - 20 °C

3.1: p-TSA / benzene / 14 h / Heating

4.1: aq. HCl / ethanol / 1.5 h / Heating

With hydrogenchloride; lithium di-tert-butyl-biphenylide; toluene-4-sulfonic acid; ozone; In tetrahydrofuran; ethanol; dichloromethane; benzene;
DOI:10.1021/ja057483x