N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N₇-[4-(phthalimido)butyl]norspermidine

Base Information

• Chemical Name: N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N₇-[4-(phthalimido)butyl]norspermidine
• CAS No.: 1154500-38-5
• Molecular Formula: C₄₁H₄₈N₄O₇
• Molecular Weight: 708.855

Synonyms:N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N₇-[4-(phthalimido)butyl]norspermidine

Chemical Property of N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N₇-[4-(phthalimido)butyl]norspermidine

Chemical Property:

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Technology Process of N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N₇-[4-(phthalimido)butyl]norspermidine

There total 1 articles about N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N₇-[4-(phthalimido)butyl]norspermidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

2,3-bis((4-methoxybenzyl)oxy)benzoic acid (1154500-36-3) + N1-[4-(phthalimido)butyl]norspermidine tris(trifluoroacetate) → N1-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N7-[4-(phthalimido)butyl]norspermidine (1154500-38-5)

Guidance literature:

2,3-bis((4-methoxybenzyl)oxy)benzoic acid; With 1,1'-carbonyldiimidazole; In dichloromethane; for 1h;

N₁-[4-(phthalimido)butyl]norspermidine tris(trifluoroacetate); With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jm900119q

Reference yield: 60.0%

N1-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N7-[4-(phthalimido)butyl]norspermidine (1154500-38-5) + N-tert-butoxycarbonyl-L-threonine N-hydroxysuccinimide ester (63076-44-8) → N4,N7-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N1-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N7-[4-(phthalimido)butyl]norspermidine (1154500-40-9)

Guidance literature:

In N,N-dimethyl-formamide; at 40 ℃; for 72h;

DOI:10.1021/jm900119q

upstream raw materials:

2,3-bis((4-methoxybenzyl)oxy)benzoic acid

Downstream raw materials:

N₄,N₇-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-[2,3-bis(4-methoxybenzyloxy)benzoyl]-N₇-[4-(phthalimido)butyl]norspermidine

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