C₂₄H₂₂N₂O₈S₂

Base Information

Chemical Name:C₂₄H₂₂N₂O₈S₂
CAS No.:1309362-07-9
Molecular Formula:C₂₄H₂₂N₂O₈S₂
Molecular Weight:530.579
Hs Code.:

C<sub>24</sub>H<sub>22</sub>N<sub>2</sub>O<sub>8</sub>S<sub>2</sub>

Synonyms:C₂₄H₂₂N₂O₈S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₂₂N₂O₈S₂

Chemical Property:

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Technology Process of C₂₄H₂₂N₂O₈S₂

There total 4 articles about C₂₄H₂₂N₂O₈S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 16629-19-9
thiophene-2-sulfonyl chloride

: 1309362-10-4
C₂₀H₂₀N₂O₆

: 1309362-07-9
C₂₄H₂₂N₂O₈S₂

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere; Cooling with ice;
DOI:10.1002/cmdc.201000489

Reference yield:

: 1677-46-9
4-hydroxy-1-methyl-2(1H)-quinolone

: 1309362-07-9
C₂₄H₂₂N₂O₈S₂

Guidance literature:: Multi-step reaction with 4 steps

1: nitric acid / acetic acid / 90 °C

2: hydrogenchloride; palladium 10% on activated carbon; hydrogen / tetrahydrofuran; water / 8 h / 20 °C / Darkness

3: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C / Inert atmosphere; Darkness

4: triethylamine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

With hydrogenchloride; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; nitric acid; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; acetic acid;
DOI:10.1002/cmdc.201000489

Reference yield:

: 36949-55-0
4-hydroxy-1-methyl-3-nitro-2-(1H)quinolinone

: 1309362-07-9
C₂₄H₂₂N₂O₈S₂

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / tetrahydrofuran; water / 8 h / 20 °C / Darkness

2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C / Inert atmosphere; Darkness

3: triethylamine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

With hydrogenchloride; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/cmdc.201000489