((2S,6R)-6-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)-4-tritylmorpholin-2-yl)methyl hexyl(methyl)phosphoramidochloridate

Base Information

Chemical Name:((2S,6R)-6-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)-4-tritylmorpholin-2-yl)methyl hexyl(methyl)phosphoramidochloridate
CAS No.:1351280-93-7
Molecular Formula:C₃₆H₄₄ClN₄O₅P
Molecular Weight:679.196
Hs Code.:

Synonyms:((2S,6R)-6-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)-4-tritylmorpholin-2-yl)methyl hexyl(methyl)phosphoramidochloridate

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Chemical Property of ((2S,6R)-6-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)-4-tritylmorpholin-2-yl)methyl hexyl(methyl)phosphoramidochloridate

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Technology Process of ((2S,6R)-6-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)-4-tritylmorpholin-2-yl)methyl hexyl(methyl)phosphoramidochloridate

There total 2 articles about ((2S,6R)-6-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)-4-tritylmorpholin-2-yl)methyl hexyl(methyl)phosphoramidochloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 914361-76-5
1-((2R,6S)-6-(hydroxymethyl)-4-tritylmorpholin-2-yl)-5-methylpyrimidine-2,4(1H,3H)-dione

: 1351280-92-6
C₇H₁₆Cl₂NOP

: 1351280-93-7
((2S,6R)-6-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)-4-tritylmorpholin-2-yl)methyl hexyl(methyl)phosphoramidochloridate

Guidance literature:: With 2,6-dimethylpyridine; dmap; In dichloromethane; at 0 - 20 ℃; for 18h;

Reference yield:

: 35161-70-7
N-methylhexanamine

: 1351280-93-7
((2S,6R)-6-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)-4-tritylmorpholin-2-yl)methyl hexyl(methyl)phosphoramidochloridate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; trichlorophosphate / dichloromethane / -78 - 20 °C / Inert atmosphere

2: 2,6-dimethylpyridine; dmap / dichloromethane / 18 h / 0 - 20 °C

With 2,6-dimethylpyridine; dmap; triethylamine; trichlorophosphate; In dichloromethane;