Technology Process of C29H14N6O2
There total 4 articles about C29H14N6O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
dimethyl sulfoxide;
at 30 ℃;
for 24h;
pH=2;
Inert atmosphere;
DOI:10.1002/pola.26331
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dicyclohexyl-carbodiimide / tetrahydrofuran / 24 h / Inert atmosphere; Cooling with ice
2: acetic acid / 16 h / 120 - 130 °C / Reflux; Inert atmosphere
3: potassium carbonate / dimethyl sulfoxide / 24 h / 30 °C / pH 2 / Inert atmosphere
With
potassium carbonate; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; acetic acid; dimethyl sulfoxide;
DOI:10.1002/pola.26331
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dicyclohexyl-carbodiimide / tetrahydrofuran / 24 h / Inert atmosphere; Cooling with ice
2: acetic acid / 16 h / 120 - 130 °C / Reflux; Inert atmosphere
3: potassium carbonate / dimethyl sulfoxide / 24 h / 30 °C / pH 2 / Inert atmosphere
With
potassium carbonate; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; acetic acid; dimethyl sulfoxide;
DOI:10.1002/pola.26331