1-carbomethoxy-7-(4-methoxybenzenesulfonyl)-1,2,3,4,4aα,5,6,11cα-octahydro-7H-pyrido<3,2,c>carbazole

Base Information

Chemical Name:1-carbomethoxy-7-(4-methoxybenzenesulfonyl)-1,2,3,4,4aα,5,6,11cα-octahydro-7H-pyrido<3,2,c>carbazole
CAS No.:81816-27-5
Molecular Formula:C₂₄H₂₆N₂O₅S
Molecular Weight:454.547
Hs Code.:

Synonyms:1-carbomethoxy-7-(4-methoxybenzenesulfonyl)-1,2,3,4,4aα,5,6,11cα-octahydro-7H-pyrido<3,2,c>carbazole

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Chemical Property of 1-carbomethoxy-7-(4-methoxybenzenesulfonyl)-1,2,3,4,4aα,5,6,11cα-octahydro-7H-pyrido<3,2,c>carbazole

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Technology Process of 1-carbomethoxy-7-(4-methoxybenzenesulfonyl)-1,2,3,4,4aα,5,6,11cα-octahydro-7H-pyrido<3,2,c>carbazole

There total 8 articles about 1-carbomethoxy-7-(4-methoxybenzenesulfonyl)-1,2,3,4,4aα,5,6,11cα-octahydro-7H-pyrido<3,2,c>carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 85923-42-8
N-<<(4-methoxybenzenesulfonyl)-2-methyl-1H-indol-3-yl>methylene>-4-pentenylamine

: 79-22-1
methyl chloroformate

: 81816-27-5
1-carbomethoxy-7-(4-methoxybenzenesulfonyl)-1,2,3,4,4aα,5,6,11cα-octahydro-7H-pyrido<3,2,c>carbazole

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In chlorobenzene; at 130 ℃; for 3.5h;
DOI:10.1016/S0040-4020(01)93262-4

Reference yield:

: 487-89-8,1228547-52-1
Indole-3-carboxaldehyde

: 81816-27-5
1-carbomethoxy-7-(4-methoxybenzenesulfonyl)-1,2,3,4,4aα,5,6,11cα-octahydro-7H-pyrido<3,2,c>carbazole

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / NaH, imidazole / various solvent(s) / 2 h / Heating

2: benzene / 1 h

3: n-BuLi / tetrahydrofuran; hexane / -78 deg C then room temp.

4: 88 percent / diisopropylethylamine / chlorobenzene / 3.5 h / 130 °C

With 1H-imidazole; n-butyllithium; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; chlorobenzene; benzene;
DOI:10.1016/S0040-4020(01)93262-4

Reference yield:

: 22537-07-1
4-pentenyl-1-amine

: 81816-27-5
1-carbomethoxy-7-(4-methoxybenzenesulfonyl)-1,2,3,4,4aα,5,6,11cα-octahydro-7H-pyrido<3,2,c>carbazole

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 1 h

2: n-BuLi / tetrahydrofuran; hexane / -78 deg C then room temp.

3: 88 percent / diisopropylethylamine / chlorobenzene / 3.5 h / 130 °C

With n-butyllithium; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; chlorobenzene; benzene;
DOI:10.1016/S0040-4020(01)93262-4