1,3-di(1-n-butyl-1,2,3-triazol-4-yl)benzene

Base Information

Chemical Name:1,3-di(1-n-butyl-1,2,3-triazol-4-yl)benzene
CAS No.:1285707-21-2
Molecular Formula:C₁₈H₂₄N₆
Molecular Weight:324.429
Hs Code.:

Synonyms:1,3-di(1-n-butyl-1,2,3-triazol-4-yl)benzene

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Chemical Property of 1,3-di(1-n-butyl-1,2,3-triazol-4-yl)benzene

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Technology Process of 1,3-di(1-n-butyl-1,2,3-triazol-4-yl)benzene

There total 1 articles about 1,3-di(1-n-butyl-1,2,3-triazol-4-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 7332-00-5
n-butylazide

: 1785-61-1
1,3-diethynylbenzene

: 1285707-21-2
1,3-di(1-n-butyl-1,2,3-triazol-4-yl)benzene

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In ethanol; water; at 20 ℃; for 24h;
DOI:10.1021/om200039j

Reference yield: 31.0%

: 17084-13-8
potassium hexafluorophosphate

: 146164-70-7
{Ru(4'-Ph-2,2':6',2''-terpyridine)Cl3}

: 1285707-21-2
1,3-di(1-n-butyl-1,2,3-triazol-4-yl)benzene

: 75-05-8,26809-02-9
acetonitrile

: 1285707-36-9
[Ru(4'-tolyl-2,2':6',2''-terpyridine)(1,3-bis(1-butyl-1H-1,2,3-triazol-4-yl)benzene)]PF₆

Guidance literature:: With silver triflate; In N,N-dimethyl-formamide; addn. of Ru(PhC5H2N(C5H4N)2)Cl3 and AgOTf to Me2CO, reflux for 3 h, cooling to room temp., filtration, concn. to dryness, addn. of C6H4(C2HN3Bu)2, DMF, reflux for 24 h, cooling to room temp., removal of solvent, dissolving in MeOH, addn. of excess KPF6; pptn., filtration, washing with H2O and Et2O, chromy. on silica gel (eluent: CH2Cl2/CH3CN, 10:1); elem. anal.;
DOI:10.1021/om200039j

Reference yield:

: 17084-13-8
potassium hexafluorophosphate

: 1285707-21-2
1,3-di(1-n-butyl-1,2,3-triazol-4-yl)benzene

: C₃₁H₃₅N₃O₄Ru⁽³⁺⁾*3CF₃O₃S^(1-)

: [(4'-p-methoxyphenyl-2,2':6',2''-terpyridine)Ru(1,3-di(N-n-butyl-1,2,3-triazol-4-yl)benzene)](PF₆)

Guidance literature:: 1,3-di(1-n-butyl-1,2,3-triazol-4-yl)benzene; C₃₁H₃₅N₃O₄Ru⁽³⁺⁾*3CF₃O₃S^(1-); In N,N-dimethyl-formamide; tert-butyl alcohol; for 24h; Reflux; Sealed tube;

potassium hexafluorophosphate; In methanol;
DOI:10.1002/cjoc.201201170