methyl O-(6-O-acetyl-3-O-benzoyl-4-O-α-D-arabino-hexopyranosyl)-(1<*>6)-3-O-benzoyl-4-O-benzyl-2-deoxy-α-D-arabino-hexapyranoside

Base Information

• Chemical Name: methyl O-(6-O-acetyl-3-O-benzoyl-4-O-α-D-arabino-hexopyranosyl)-(1<*>6)-3-O-benzoyl-4-O-benzyl-2-deoxy-α-D-arabino-hexapyranoside
• CAS No.: 164664-79-3
• Molecular Formula: C₄₃H₄₆O₁₂
• Molecular Weight: 754.831

Synonyms:methyl O-(6-O-acetyl-3-O-benzoyl-4-O-α-D-arabino-hexopyranosyl)-(1<*>6)-3-O-benzoyl-4-O-benzyl-2-deoxy-α-D-arabino-hexapyranoside

Chemical Property of methyl O-(6-O-acetyl-3-O-benzoyl-4-O-α-D-arabino-hexopyranosyl)-(1<*>6)-3-O-benzoyl-4-O-benzyl-2-deoxy-α-D-arabino-hexapyranoside

Chemical Property:

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Safty Information:

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Technology Process of methyl O-(6-O-acetyl-3-O-benzoyl-4-O-α-D-arabino-hexopyranosyl)-(1<*>6)-3-O-benzoyl-4-O-benzyl-2-deoxy-α-D-arabino-hexapyranoside

There total 1 articles about methyl O-(6-O-acetyl-3-O-benzoyl-4-O-α-D-arabino-hexopyranosyl)-(1<*>6)-3-O-benzoyl-4-O-benzyl-2-deoxy-α-D-arabino-hexapyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-O-acetyl-3-O-benzoyl-4-O-benzyl-1-O-tert-butyldimethylsilyl-2-deoxy-β-D-arabino-hexopyranose (164664-74-8) + methyl 3-O-benzoyl-4-O-benzyl-2-deoxy-α-D-arabino-hexopyranoside (164664-73-7) → methyl O-(6-O-acetyl-3-O-benzoyl-4-O-α-D-arabino-hexopyranosyl)-(1<*>6)-3-O-benzoyl-4-O-benzyl-2-deoxy-α-D-arabino-hexapyranoside (164664-79-3)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; Yield given. Multistep reaction; 1.) CH₂Cl₂, 30 min, 2.) CH₂Cl₂, -50 deg C, 14 h;

DOI:10.1016/0008-6215(94)00314-6

Reference yield: 92.0%

methyl O-(6-O-acetyl-3-O-benzoyl-4-O-α-D-arabino-hexopyranosyl)-(1<*>6)-3-O-benzoyl-4-O-benzyl-2-deoxy-α-D-arabino-hexapyranoside (164664-79-3) → methyl O-(4-O-benzyl-2-deoxy-α-D-arabino-hexopyranosyl)-(1<*>6)-4-O-benzyl-2-deoxy-α-D-arabino-hexapyranoside

Guidance literature:

With sodium methylate; In methanol; toluene; Ambient temperature;

DOI:10.1016/0008-6215(94)00314-6

Reference yield: 90.0%

methyl O-(6-O-acetyl-3-O-benzoyl-4-O-α-D-arabino-hexopyranosyl)-(1<*>6)-3-O-benzoyl-4-O-benzyl-2-deoxy-α-D-arabino-hexapyranoside (164664-79-3) → methyl O-(3-O-benzoyl-4-O-benzyl-2-deoxy-α-D-arabino-hexopyranosyl)-(1<*>6)-3-O-benzoyl-4-O-benzyl-2-deoxy-α-D-arabino-hexopyranoside

Guidance literature:

With sodium methylate; In methanol; toluene; for 1h; Ambient temperature;

DOI:10.1016/0008-6215(94)00315-7

upstream raw materials:

6-O-acetyl-3-O-benzoyl-4-O-benzyl-1-O-tert-butyldimethylsilyl-2-deoxy-β-D-arabino-hexopyranose

methyl 3-O-benzoyl-4-O-benzyl-2-deoxy-α-D-arabino-hexopyranoside

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