5-(4-methylphenyl)-5,6,7,8-tetrahydroimidazo<1,5-a>pyridine hydrochloride

Base Information

Chemical Name:5-(4-methylphenyl)-5,6,7,8-tetrahydroimidazo<1,5-a>pyridine hydrochloride
CAS No.:102676-44-8
Molecular Formula:C₁₄H₁₆N₂*ClH
Molecular Weight:248.755
Hs Code.:

Synonyms:5-(4-methylphenyl)-5,6,7,8-tetrahydroimidazo<1,5-a>pyridine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(4-methylphenyl)-5,6,7,8-tetrahydroimidazo<1,5-a>pyridine hydrochloride

Chemical Property:

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Technology Process of 5-(4-methylphenyl)-5,6,7,8-tetrahydroimidazo<1,5-a>pyridine hydrochloride

There total 2 articles about 5-(4-methylphenyl)-5,6,7,8-tetrahydroimidazo<1,5-a>pyridine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 131833-71-1
5-<4-(hydroxymethyl)phenyl>-5,6,7,8-tetrahydroimidazo<1,5-a>pyridine

: 102676-44-8
5-(4-methylphenyl)-5,6,7,8-tetrahydroimidazo<1,5-a>pyridine hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; at 60 ℃; for 4h; under 2068.6 Torr;
DOI:10.1021/jm00106a038

Reference yield:

: 131833-88-0
5-<4-(ethoxycarbonyl)phenyl>-5,6,7,8-tetrahydroimidazo<1,5-a>pyridine

: 102676-44-8
5-(4-methylphenyl)-5,6,7,8-tetrahydroimidazo<1,5-a>pyridine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / diisobutylaluminum hydride / CH₂Cl₂; toluene / -70 - 20 °C

2: 63 percent / H₂, conc. HCl / 10percent Pd/C / ethanol / 4 h / 60 °C / 2068.6 Torr

With hydrogenchloride; hydrogen; diisobutylaluminium hydride; palladium on activated charcoal; In ethanol; dichloromethane; toluene;
DOI:10.1021/jm00106a038