1,4-bis-{5'-[(N',N''-t-butoxycarbonyl)guanidino]pyridin-2'-yl}phenylene

Base Information

• Chemical Name: 1,4-bis-{5'-[(N',N''-t-butoxycarbonyl)guanidino]pyridin-2'-yl}phenylene
• CAS No.: 1104620-30-5
• Molecular Formula: C₃₈H₅₀N₈O₈
• Molecular Weight: 746.864

Synonyms:1,4-bis-{5'-[(N',N''-t-butoxycarbonyl)guanidino]pyridin-2'-yl}phenylene

Chemical Property of 1,4-bis-{5'-[(N',N''-t-butoxycarbonyl)guanidino]pyridin-2'-yl}phenylene

Chemical Property:

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Technology Process of 1,4-bis-{5'-[(N',N''-t-butoxycarbonyl)guanidino]pyridin-2'-yl}phenylene

There total 1 articles about 1,4-bis-{5'-[(N',N''-t-butoxycarbonyl)guanidino]pyridin-2'-yl}phenylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1,4-bis-[5'-aminopyridin-2'-yl]phenylene (916653-41-3) + N,N'-bis-Boc-S-methyl-isothiourea (322474-21-5) → 1,4-bis-{5'-[(N',N''-t-butoxycarbonyl)guanidino]pyridin-2'-yl}phenylene (1104620-30-5)

Guidance literature:

With triethylamine; mercury dichloride; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

DOI:10.1016/j.ejmech.2008.02.008

Reference yield: 55.0%

1,4-bis-{5'-[(N',N''-t-butoxycarbonyl)guanidino]pyridin-2'-yl}phenylene (1104620-30-5) → 1,4-bis-[5'-guanidinopyridin-2'-yl]phenylene tetrahydrochloride

Guidance literature:

With hydrogenchloride; ethanol; In dichloromethane; at 20 ℃; for 72h;

DOI:10.1016/j.ejmech.2008.02.008

upstream raw materials:

1,4-bis-[5'-aminopyridin-2'-yl]phenylene

N,N'-bis-Boc-S-methyl-isothiourea

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