N-benzyl(2-(3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl)-4-methoxyphenyl)carbamoyl cyanide

Base Information

Chemical Name:N-benzyl(2-(3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl)-4-methoxyphenyl)carbamoyl cyanide
CAS No.:1208117-66-1
Molecular Formula:C₂₅H₃₂N₂O₃Si
Molecular Weight:436.626
Hs Code.:

Synonyms:N-benzyl(2-(3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl)-4-methoxyphenyl)carbamoyl cyanide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl(2-(3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl)-4-methoxyphenyl)carbamoyl cyanide

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Technology Process of N-benzyl(2-(3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl)-4-methoxyphenyl)carbamoyl cyanide

There total 1 articles about N-benzyl(2-(3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl)-4-methoxyphenyl)carbamoyl cyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1115-12-4
carbonyl cyanide

: 1208117-86-5
C₂₃H₃₃NO₂Si

: 1208117-66-1
N-benzyl(2-(3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl)-4-methoxyphenyl)carbamoyl cyanide

Guidance literature:: In diethyl ether; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol902949d

Reference yield: 88.0%

: 1208117-66-1
N-benzyl(2-(3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl)-4-methoxyphenyl)carbamoyl cyanide

: 1208117-67-2
(S)-2-(1-benzyl-3-((tert-butyldimethylsilyloxy)methyl)-5-methoxy-2-oxoindolin-3-yl)acetonitrile

Guidance literature:: With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (R)-5,5’,6,6’,7,7’,8,8’-octahydro-1,1-binaphthylphosphinite diisopropylamidite; In tetrahydrofuran; at 100 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Glove box;
DOI:10.1021/ol902949d