[(1,3-phenylene)bis(methylene)]-(1-ethylimidazolium)-(3-ethyl-imidazol-2-thione) chloride

Base Information

• Chemical Name: [(1,3-phenylene)bis(methylene)]-(1-ethylimidazolium)-(3-ethyl-imidazol-2-thione) chloride
• CAS No.: 1166834-07-6
• Molecular Formula: C₁₈H₂₃N₄S*Cl
• Molecular Weight: 362.926
• Mol file: 1166834-07-6.mol

Synonyms:[(1,3-phenylene)bis(methylene)]-(1-ethylimidazolium)-(3-ethyl-imidazol-2-thione) chloride

Chemical Property of [(1,3-phenylene)bis(methylene)]-(1-ethylimidazolium)-(3-ethyl-imidazol-2-thione) chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of [(1,3-phenylene)bis(methylene)]-(1-ethylimidazolium)-(3-ethyl-imidazol-2-thione) chloride

There total 1 articles about [(1,3-phenylene)bis(methylene)]-(1-ethylimidazolium)-(3-ethyl-imidazol-2-thione) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

[(1,3-phenylene)bis(methylene)]bis(1-ethyl-imidazol-2-ylidene) (1166834-03-2) → [(1,3-phenylene)bis(methylene)]bis(1-ethylimidazol-2-thione) (1166834-08-7) + [(1,3-phenylene)bis(methylene)]-(1-ethylimidazolium)-(3-ethyl-imidazol-2-thione) chloride (1166834-07-6)

Guidance literature:

With sulfur; lithium chloride; In methanol; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1039/b902733e

Reference yield: 100.0%

[(1,3-phenylene)bis(methylene)]-(1-ethylimidazolium)-(3-ethyl-imidazol-2-thione) chloride (1166834-07-6) → [(1,3-phenylene)bis(methylene)]bis(1-ethylimidazol-2-thione) (1166834-08-7)

Guidance literature:

With caesium carbonate; sulfur; In methanol; at 20 ℃; for 15h; Inert atmosphere;

DOI:10.1039/b902733e

upstream raw materials:

[(1,3-phenylene)bis(methylene)]bis(1-ethyl-imidazol-2-ylidene)

Downstream raw materials:

[(1,3-phenylene)bis(methylene)]bis(1-ethylimidazol-2-thione)