C₄₈H₄₇BrN₄O₈Zn

Base Information Edit

Chemical Name:C₄₈H₄₇BrN₄O₈Zn
CAS No.:1062503-88-1
Molecular Formula:C₄₈H₄₇BrN₄O₈Zn
Molecular Weight:953.217
Hs Code.:
Mol file:1062503-88-1.mol

C<sub>48</sub>H<sub>47</sub>BrN<sub>4</sub>O<sub>8</sub>Zn

Synonyms:C₄₈H₄₇BrN₄O₈Zn

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Chemical Property of C₄₈H₄₇BrN₄O₈Zn Edit

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Technology Process of C₄₈H₄₇BrN₄O₈Zn

There total 7 articles about C₄₈H₄₇BrN₄O₈Zn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1051971-73-3
C₆₆H₈₅BrN₄O₈SiZn

: 1062503-88-1
C₄₈H₄₇BrN₄O₈Zn

Guidance literature:: C₆₆H₈₅BrN₄O₈SiZn; With tetrabutyl ammonium fluoride; In dichloromethane; at 20 ℃; for 0.25h;

With calcium chloride; In dichloromethane; at 20 ℃; for 0.166667h;

Reference yield:

: 1051971-73-3
Zn((MeO(CH₂CH₂O)3C₆H₄)2(THSCC)(Br)C₂₀H₈N₂)

: 1062503-88-1
Zn((MeO(CH₂CH₂O)3C₆H₄)2(HCC)(Br)C₂₀H₈N₂)

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; (inert atm.); addn. of THF soln. of fluoride salt to CH2Cl2 soln. of porphyrin deriv., stirring at room temp. for 15 min; addn. of anhyd. CaCl2, stirring for 10 min, filtration, evapn., drying in vac.;
DOI:10.1039/b814789b

Reference yield:

: 1051971-71-1
5,15-bis-(3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}phenyl)porphyrin zinc

: 1062503-88-1
C₄₈H₄₇BrN₄O₈Zn

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / chloroform / 0.75 h

2.1: triethylamine; triphenylphosphine / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide / toluene / 3 h / 20 - 40 °C

3.1: tetrabutyl ammonium fluoride / dichloromethane / 0.25 h / 20 °C

3.2: 0.17 h / 20 °C

With pyridine; tetrabutyl ammonium fluoride; triethylamine; triphenylphosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; In dichloromethane; chloroform; toluene; 2.1: Sonogashira Coupling;