N-(fluoren-9-ylmethoxycarbonyl)-2-O-acetyl-3,4-di-O-benzyl-6-O-trityl-β-D-glucopyranosylamine

Base Information

Chemical Name:N-(fluoren-9-ylmethoxycarbonyl)-2-O-acetyl-3,4-di-O-benzyl-6-O-trityl-β-D-glucopyranosylamine
CAS No.:193154-25-5
Molecular Formula:C₅₆H₅₁NO₈
Molecular Weight:866.023
Hs Code.:

Synonyms:N-(fluoren-9-ylmethoxycarbonyl)-2-O-acetyl-3,4-di-O-benzyl-6-O-trityl-β-D-glucopyranosylamine

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Chemical Property of N-(fluoren-9-ylmethoxycarbonyl)-2-O-acetyl-3,4-di-O-benzyl-6-O-trityl-β-D-glucopyranosylamine

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Technology Process of N-(fluoren-9-ylmethoxycarbonyl)-2-O-acetyl-3,4-di-O-benzyl-6-O-trityl-β-D-glucopyranosylamine

There total 3 articles about N-(fluoren-9-ylmethoxycarbonyl)-2-O-acetyl-3,4-di-O-benzyl-6-O-trityl-β-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 193154-24-4
2-O-acetyl-3,4-di-O-benzyl-6-O-trityl-β-D-glucopyranosylamine

: 193154-25-5
N-(fluoren-9-ylmethoxycarbonyl)-2-O-acetyl-3,4-di-O-benzyl-6-O-trityl-β-D-glucopyranosylamine

Guidance literature:: With sodium hydrogencarbonate; sodium carbonate; In 1,4-dioxane; for 3h;
DOI:10.1002/chem.19970030614

Reference yield:

: 169824-26-4
1,2-anhydro-3,4-di-O-benzyl-6-O-trityl-α-D-glucopyranoside

: 193154-25-5
N-(fluoren-9-ylmethoxycarbonyl)-2-O-acetyl-3,4-di-O-benzyl-6-O-trityl-β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / ZnCl₂ / tetrahydrofuran / 2 h

2: aq. H₂SO₄ / tetrahydrofuran / 0.5 h

3: 87 percent / aq. NaHCO₃, Na₂CO₃ / dioxane / 3 h

With sulfuric acid; sodium hydrogencarbonate; sodium carbonate; zinc(II) chloride; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1002/chem.19970030614

Reference yield:

: 193154-23-3
(3aS,5R,6R,7S,7aR)-6,7-Bis-benzyloxy-2-methyl-5-trityloxymethyl-5,6,7,7a-tetrahydro-3aH-pyrano[2,3-d]oxazole

: 193154-25-5
N-(fluoren-9-ylmethoxycarbonyl)-2-O-acetyl-3,4-di-O-benzyl-6-O-trityl-β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: aq. H₂SO₄ / tetrahydrofuran / 0.5 h

2: 87 percent / aq. NaHCO₃, Na₂CO₃ / dioxane / 3 h

With sulfuric acid; sodium hydrogencarbonate; sodium carbonate; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1002/chem.19970030614