C₂₅H₂₂O₃

Base Information

Chemical Name:C₂₅H₂₂O₃
CAS No.:1353653-26-5
Molecular Formula:C₂₅H₂₂O₃
Molecular Weight:370.448
Hs Code.:

C<sub>25</sub>H<sub>22</sub>O<sub>3</sub>

Synonyms:C₂₅H₂₂O₃

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Chemical Property of C₂₅H₂₂O₃

Chemical Property:

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Technology Process of C₂₅H₂₂O₃

There total 3 articles about C₂₅H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353653-23-2
C₂₀H₂₂O₂

: 1353653-26-5
C₂₅H₂₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 16 h / 20 °C

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 3 h / Reflux; Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; triethylamine; In dichloromethane;
DOI:10.1016/j.tet.2011.10.023

Reference yield:

: 1353653-22-1
C₂₂H₂₄O₃

: 1353653-26-5
C₂₅H₂₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / hexanes; dichloromethane / 2 h / -78 °C

1.2: Saturated solution; Cooling with ice

2.1: dmap; triethylamine / dichloromethane / 16 h / 20 °C

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 3 h / Reflux; Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; diisobutylaluminium hydride; triethylamine; In hexanes; dichloromethane;
DOI:10.1016/j.tet.2011.10.023

Reference yield:

: 4165-79-1
1,1-diphenyl-3-buten-1-ol

: 1353653-26-5
C₂₅H₂₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C

1.2: 1 h / 0 - 20 °C

2.1: diisobutylaluminium hydride / hexanes; dichloromethane / 2 h / -78 °C

2.2: Saturated solution; Cooling with ice

3.1: dmap; triethylamine / dichloromethane / 16 h / 20 °C

4.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 3 h / Reflux; Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; potassium hydride; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; hexanes; dichloromethane; mineral oil;
DOI:10.1016/j.tet.2011.10.023