acetic acid 2-methoxy-1-(2-oxopiperidin-3-yl)-2-phenylsulfanyl ethyl ester

Base Information

• Chemical Name: acetic acid 2-methoxy-1-(2-oxopiperidin-3-yl)-2-phenylsulfanyl ethyl ester
• CAS No.: 420131-61-9
• Molecular Formula: C₁₆H₂₁NO₄S
• Molecular Weight: 323.413

Synonyms:acetic acid 2-methoxy-1-(2-oxopiperidin-3-yl)-2-phenylsulfanyl ethyl ester

Chemical Property of acetic acid 2-methoxy-1-(2-oxopiperidin-3-yl)-2-phenylsulfanyl ethyl ester

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Technology Process of acetic acid 2-methoxy-1-(2-oxopiperidin-3-yl)-2-phenylsulfanyl ethyl ester

There total 1 articles about acetic acid 2-methoxy-1-(2-oxopiperidin-3-yl)-2-phenylsulfanyl ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

1-(trimethylsilyl)piperidin-2-one (3553-93-3) + acetic anhydride (108-24-7) + methoxyphenylsulfanyl acetaldehyde (94633-78-0) → acetic acid 2-methoxy-1-(2-oxopiperidin-3-yl)-2-phenylsulfanyl ethyl ester (420131-61-9)

Guidance literature:

1-(trimethylsilyl)piperidin-2-one; methoxyphenylsulfanyl acetaldehyde; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -75 ℃; for 0.5h;

acetic anhydride; In tetrahydrofuran; hexane; at -75 - 20 ℃;

DOI:10.1139/cjc-79-11-1681

Reference yield: 94.0%

but-3-enoyl chloride (1470-91-3) + acetic acid 2-methoxy-1-(2-oxopiperidin-3-yl)-2-phenylsulfanyl ethyl ester (420131-61-9) → acetic acid 1-(1-but-3-enoyl-2-oxopiperidin-3-yl)-2-methoxy-2-phenylsulfanyl ethyl ester

Guidance literature:

With molecular sieve; In dichloromethane; at 20 ℃;

DOI:10.1139/cjc-79-11-1681

upstream raw materials:

1-(trimethylsilyl)piperidin-2-one

acetic anhydride

methoxyphenylsulfanyl acetaldehyde

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