ethyl 3-methyl-5-phenyl-2-thiophenecarboxylate

Base Information

Chemical Name:ethyl 3-methyl-5-phenyl-2-thiophenecarboxylate
CAS No.:23806-18-0
Molecular Formula:C₁₄H₁₄O₂S
Molecular Weight:246.33
Hs Code.:

Synonyms:ethyl 3-methyl-5-phenyl-2-thiophenecarboxylate

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Chemical Property of ethyl 3-methyl-5-phenyl-2-thiophenecarboxylate

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Technology Process of ethyl 3-methyl-5-phenyl-2-thiophenecarboxylate

There total 3 articles about ethyl 3-methyl-5-phenyl-2-thiophenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 91667-27-5
(Z)-4-chloro-4-phenylbut-3-en-2-one

: 55163-91-2
ethyl thioglycolate sodium salt

: 23806-18-0
ethyl 3-methyl-5-phenyl-2-thiophenecarboxylate

Guidance literature:: In ethanol; Heating;

Reference yield: 69.0%

: ethyl 2-(N-tosylhydrazono)acetate

: (E)-3-(benzylamino)-3-ethoxy-1-phenylprop-2-ene-1-thione

: 23806-18-0
ethyl 3-methyl-5-phenyl-2-thiophenecarboxylate

Guidance literature:: With lithium tert-butoxide; In 1,4-dioxane; at 110 ℃; for 3h; chemoselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201801028

Reference yield:

: 23806-18-0
ethyl 3-methyl-5-phenyl-2-thiophenecarboxylate

Guidance literature:: aus 2-Aethoxycarbonyl-5-phenyl-3-methyl-3-hydroxy-tetrahydro-thiophen mit Poly- phosphorsaeure (20grad, 30 Min.; 95grad, 4 Std.);

upstream raw materials:

(Z)-4-chloro-4-phenylbut-3-en-2-one

ethyl thioglycolate sodium salt

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