2-(trimethylsilyl)ethyl (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-acetamido-6-O-[(S)-1-benzoxycarbonyl-2-phenyl-ethyl]-2-deoxy-β-D-galactopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-acetamido-6-O-[(S)-1-benzoxycarbonyl-2-phenyl-ethyl]-2-deoxy-β-D-galactopyranoside
CAS No.:1123178-65-3
Molecular Formula:C₇₂H₉₀N₂O₂₈Si
Molecular Weight:1459.59
Hs Code.:

2-(trimethylsilyl)ethyl (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-acetamido-6-O-[(S)-1-benzoxycarbonyl-2-phenyl-ethyl]-2-deoxy-β-D-galactopyranoside

Synonyms:2-(trimethylsilyl)ethyl (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-acetamido-6-O-[(S)-1-benzoxycarbonyl-2-phenyl-ethyl]-2-deoxy-β-D-galactopyranoside

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Chemical Property of 2-(trimethylsilyl)ethyl (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-acetamido-6-O-[(S)-1-benzoxycarbonyl-2-phenyl-ethyl]-2-deoxy-β-D-galactopyranoside

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Technology Process of 2-(trimethylsilyl)ethyl (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-acetamido-6-O-[(S)-1-benzoxycarbonyl-2-phenyl-ethyl]-2-deoxy-β-D-galactopyranoside

There total 1 articles about 2-(trimethylsilyl)ethyl (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-acetamido-6-O-[(S)-1-benzoxycarbonyl-2-phenyl-ethyl]-2-deoxy-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1123178-63-1
2-(trimethylsilyl)ethyl (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-6-O-[(S)-1-benzoxycarbonyl-2-phenyl-ethyl]-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

: 1123178-65-3
2-(trimethylsilyl)ethyl (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-acetamido-6-O-[(S)-1-benzoxycarbonyl-2-phenyl-ethyl]-2-deoxy-β-D-galactopyranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; at 20 ℃; for 3.75h; Inert atmosphere; Reflux;
DOI:10.1021/jm801058n

Reference yield: 87.0%

: 1123178-65-3
2-(trimethylsilyl)ethyl (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-acetamido-6-O-[(S)-1-benzoxycarbonyl-2-phenyl-ethyl]-2-deoxy-β-D-galactopyranoside

: 2-(trimethylsilyl)ethyl (sodium 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-β-D-galactopyranosyl-(1->3)-2-acetamido-2-deoxy-6-O-[sodium (S)-1-carboxylato-2-phenyl-ethyl]-β-D-galactopyranoside

Guidance literature:: 2-(trimethylsilyl)ethyl (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-acetamido-6-O-[(S)-1-benzoxycarbonyl-2-phenyl-ethyl]-2-deoxy-β-D-galactopyranoside; With methanol; sodium methylate; at 20 ℃; for 19h; Inert atmosphere;

With water; In methanol; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jm801058n