N-α-Boc-N-ε-EDTA(Bn)3-L-Lys-O-Tmse ester

Base Information

Chemical Name:N-α-Boc-N-ε-EDTA(Bn)3-L-Lys-O-Tmse ester
CAS No.:134020-69-2
Molecular Formula:C₄₇H₆₆N₄O₁₁Si
Molecular Weight:891.147
Hs Code.:

Synonyms:N-α-Boc-N-ε-EDTA(Bn)3-L-Lys-O-Tmse ester

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Chemical Property of N-α-Boc-N-ε-EDTA(Bn)3-L-Lys-O-Tmse ester

Chemical Property:

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Technology Process of N-α-Boc-N-ε-EDTA(Bn)3-L-Lys-O-Tmse ester

There total 5 articles about N-α-Boc-N-ε-EDTA(Bn)3-L-Lys-O-Tmse ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 134020-68-1
N-α-Boc-L-Lys-O-Tmse ester

: 134020-65-8
Tribenzyl EDTA

: 134020-69-2
N-α-Boc-N-ε-EDTA(Bn)3-L-Lys-O-Tmse ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 23h; Ambient temperature;
DOI:10.1016/S0040-4020(01)81787-7

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 134020-69-2
N-α-Boc-N-ε-EDTA(Bn)3-L-Lys-O-Tmse ester

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (EDCI), 4-dimethylaminopyridine (DMAP) / CH₂Cl₂ / 12 h / Ambient temperature

2: 94 percent / piperidine / 2 h / Ambient temperature

3: 91 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (EDCI), 4-dimethylaminopyridine (DMAP) / CH₂Cl₂ / 23 h / Ambient temperature

With piperidine; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1016/S0040-4020(01)81787-7

Reference yield:

: 84624-27-1
Boc-Lys(Fmoc)-OH

: 134020-69-2
N-α-Boc-N-ε-EDTA(Bn)3-L-Lys-O-Tmse ester

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (EDCI), 4-dimethylaminopyridine (DMAP) / CH₂Cl₂ / 12 h / Ambient temperature

2: 94 percent / piperidine / 2 h / Ambient temperature

3: 91 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (EDCI), 4-dimethylaminopyridine (DMAP) / CH₂Cl₂ / 23 h / Ambient temperature

With piperidine; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1016/S0040-4020(01)81787-7