Thioacetic acid S-[4-(4-acetylsulfanylmethyl-benzylsulfanylmethyl)-benzyl] ester

Base Information

• Chemical Name: Thioacetic acid S-[4-(4-acetylsulfanylmethyl-benzylsulfanylmethyl)-benzyl] ester
• CAS No.: 144852-41-5
• Molecular Formula: C₂₀H₂₂O₂S₃
• Molecular Weight: 390.591

Synonyms:Thioacetic acid S-[4-(4-acetylsulfanylmethyl-benzylsulfanylmethyl)-benzyl] ester

Chemical Property of Thioacetic acid S-[4-(4-acetylsulfanylmethyl-benzylsulfanylmethyl)-benzyl] ester

Chemical Property:

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Technology Process of Thioacetic acid S-[4-(4-acetylsulfanylmethyl-benzylsulfanylmethyl)-benzyl] ester

There total 2 articles about Thioacetic acid S-[4-(4-acetylsulfanylmethyl-benzylsulfanylmethyl)-benzyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

thioacetic acid (S)-(4-bromomethylbenzyl) ester (144852-54-0) → Thioacetic acid S-[4-(4-acetylsulfanylmethyl-benzylsulfanylmethyl)-benzyl] ester (144852-41-5)

Guidance literature:

With sodium sulfide; In acetone; Ambient temperature;

Reference yield:

1,4-bis(bromomethyl)benzene (623-24-5) → Thioacetic acid S-[4-(4-acetylsulfanylmethyl-benzylsulfanylmethyl)-benzyl] ester (144852-41-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 35 percent / DBU / tetrahydrofuran / Ambient temperature

2: 93 percent / Na₂S / acetone / Ambient temperature

With sodium sulfide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; acetone;

Reference yield: 91.0%

Thioacetic acid S-[4-(4-acetylsulfanylmethyl-benzylsulfanylmethyl)-benzyl] ester (144852-41-5) + 5-(4-bromomethylphenyl)-10,15,20-tri-p-tolylporphyrin (137759-21-8) → C112H90N8S3 (144852-44-8)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; methanol; Ambient temperature;

upstream raw materials:

thioacetic acid (S)-(4-bromomethylbenzyl) ester

1,4-bis(bromomethyl)benzene

Downstream raw materials:

(4-{4-[4-(4-Hydroxymethyl-benzylsulfanylmethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-phenyl)-methanol

C₁₁₂H₉₀N₈S₃

Thioacetic acid S-(4-{4-[4-(4-acetylsulfanylmethyl-benzylsulfanylmethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzyl) ester

Methanesulfonic acid 4-{4-[4-(4-methanesulfonyloxymethyl-benzylsulfanylmethyl)-benzylsulfanylmethyl]-benzylsulfanylmethyl}-benzyl ester

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