(3E)-pentadecenyl phenyl sulfone

Base Information

Chemical Name:(3E)-pentadecenyl phenyl sulfone
CAS No.:410082-75-6
Molecular Formula:C₂₁H₃₄O₂S
Molecular Weight:350.566
Hs Code.:

Synonyms:(3E)-pentadecenyl phenyl sulfone

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Chemical Property of (3E)-pentadecenyl phenyl sulfone

Chemical Property:

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Technology Process of (3E)-pentadecenyl phenyl sulfone

There total 4 articles about (3E)-pentadecenyl phenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 3112-85-4
methylphenylsulfonate

: 410082-66-5
(E)-1-bromo-2-tetradecene

: 410082-75-6
(3E)-pentadecenyl phenyl sulfone

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1021/jo0162639

Reference yield:

: 112-54-9
Dodecanal

: 410082-75-6
(3E)-pentadecenyl phenyl sulfone

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / LiBr; Et₃N / tetrahydrofuran / 20 °C

2: 90 percent / DIBAl-H / tetrahydrofuran; toluene / 1 h / -78 °C

3: 93 percent / N-bromosuccinimide; Ph₃P / CH₂Cl₂ / 2 h / 0 - 20 °C

4: 50 percent / n-butyllithium / tetrahydrofuran; hexane / -78 - 20 °C

With N-Bromosuccinimide; n-butyllithium; diisobutylaluminium hydride; triethylamine; triphenylphosphine; lithium bromide; In tetrahydrofuran; hexane; dichloromethane; toluene; 1: Horner-Wadsworth-Emmons reaction / 3: Mitsunobu reaction;
DOI:10.1021/jo0162639

Reference yield:

: 75039-86-0
(E)-Tetradec-2-en-1-ol

: 410082-75-6
(3E)-pentadecenyl phenyl sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / N-bromosuccinimide; Ph₃P / CH₂Cl₂ / 2 h / 0 - 20 °C

2: 50 percent / n-butyllithium / tetrahydrofuran; hexane / -78 - 20 °C

With N-Bromosuccinimide; n-butyllithium; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane; 1: Mitsunobu reaction;
DOI:10.1021/jo0162639