Fe⁽³⁺⁾*Cl^(1-)*(NC₂H₄)3(CH₂C₆H₂(OCH₃)(C(CH₃)3)O)2C₂H₅^(2-)=[Fe((NC₂H₄)3(CH₂C₆H₂(OCH₃)(C(CH₃)3)O)2C₂H₅)Cl]

Base Information

• Chemical Name: Fe⁽³⁺⁾*Cl^(1-)*(NC₂H₄)3(CH₂C₆H₂(OCH₃)(C(CH₃)3)O)2C₂H₅^(2-)=[Fe((NC₂H₄)3(CH₂C₆H₂(OCH₃)(C(CH₃)3)O)2C₂H₅)Cl]
• CAS No.: 204400-49-7
• Molecular Formula: C₃₂H₄₉N₃O₄*Cl*Fe
• Molecular Weight: 631.059
• Mol file: 204400-49-7.mol

Synonyms:Fe⁽³⁺⁾*Cl^(1-)*(NC₂H₄)3(CH₂C₆H₂(OCH₃)(C(CH₃)3)O)2C₂H₅^(2-)=[Fe((NC₂H₄)3(CH₂C₆H₂(OCH₃)(C(CH₃)3)O)2C₂H₅)Cl]

Chemical Property of Fe⁽³⁺⁾*Cl^(1-)*(NC₂H₄)3(CH₂C₆H₂(OCH₃)(C(CH₃)3)O)2C₂H₅^(2-)=[Fe((NC₂H₄)3(CH₂C₆H₂(OCH₃)(C(CH₃)3)O)2C₂H₅)Cl]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Fe⁽³⁺⁾*Cl^(1-)*(NC₂H₄)3(CH₂C₆H₂(OCH₃)(C(CH₃)3)O)2C₂H₅^(2-)=[Fe((NC₂H₄)3(CH₂C₆H₂(OCH₃)(C(CH₃)3)O)2C₂H₅)Cl]

There total 1 articles about Fe⁽³⁺⁾*Cl^(1-)*(NC₂H₄)3(CH₂C₆H₂(OCH₃)(C(CH₃)3)O)2C₂H₅^(2-)=[Fe((NC₂H₄)3(CH₂C₆H₂(OCH₃)(C(CH₃)3)O)2C₂H₅)Cl] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

1-ethyl-4,7-bis(3-tert-butyl-5-methoxy-2-hydroxybenzyl)-1,4,7-triazacyclononane (253669-68-0) + iron(II) chloride → Fe(3+)*Cl(1-)*(NC2H4)3(CH2C6H2(OCH3)(C(CH3)3)O)2C2H5(2-)=[Fe((NC2H4)3(CH2C6H2(OCH3)(C(CH3)3)O)2C2H5)Cl] (204400-49-7)

Guidance literature:

With air; In methanol; Fe-salt addn. to org. acid soln., stirring few min at room temp. in air, microcrystalline pptn. within a few h; ppt. filtration off, recrystn. from methanol; elem. anal.;

DOI:10.1021/ja972269x

Reference yield:

Fe(3+)*Cl(1-)*(NC2H4)3(CH2C6H2(OCH3)(C(CH3)3)O)2C2H5(2-)=[Fe((NC2H4)3(CH2C6H2(OCH3)(C(CH3)3)O)2C2H5)Cl] (204400-49-7) → Fe(3+)*Cl(1-)*(NC2H4)3(CH2C6H2(OCH3)(C(CH3)3)O)2C2H5(1-)=[Fe((NC2H4)3(CH2C6H2(OCH3)(C(CH3)3)O)2C2H5)Cl](1+)

Guidance literature:

In acetonitrile; Electrochem. Process; controlled-potential coulometry in soln. containing 0.1 M N(n-Bu)4PF6 as supporting electrolyte;

DOI:10.1021/ja972269x

upstream raw materials:

1-ethyl-4,7-bis(3-tert-butyl-5-methoxy-2-hydroxybenzyl)-1,4,7-triazacyclononane