3,4-dichloro-N'-(3-(4-(methylsulfonamido)phenyl)propanoyl)benzohydrazide

Base Information

Chemical Name:3,4-dichloro-N'-(3-(4-(methylsulfonamido)phenyl)propanoyl)benzohydrazide
CAS No.:1192365-92-6
Molecular Formula:C₁₇H₁₇Cl₂N₃O₄S
Molecular Weight:430.312
Hs Code.:

Synonyms:3,4-dichloro-N'-(3-(4-(methylsulfonamido)phenyl)propanoyl)benzohydrazide

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Chemical Property of 3,4-dichloro-N'-(3-(4-(methylsulfonamido)phenyl)propanoyl)benzohydrazide

Chemical Property:

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Technology Process of 3,4-dichloro-N'-(3-(4-(methylsulfonamido)phenyl)propanoyl)benzohydrazide

There total 4 articles about 3,4-dichloro-N'-(3-(4-(methylsulfonamido)phenyl)propanoyl)benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 51-44-5
3,4-dichlorbenzoic acid

: 1192365-88-0
3-(4-(methylsulfonamido)phenyl)propanehydrazide

: 1192365-92-6
3,4-dichloro-N'-(3-(4-(methylsulfonamido)phenyl)propanoyl)benzohydrazide

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1016/j.bmc.2009.05.085

Reference yield:

: 1097213-41-6
methyl 3-(4-(methylsulfonamido)phenyl)propanoate

: 1192365-92-6
3,4-dichloro-N'-(3-(4-(methylsulfonamido)phenyl)propanoyl)benzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / 12 h / Reflux

2: dicyclohexyl-carbodiimide / dichloromethane; N,N-dimethyl-formamide / 12 h / 20 °C

With hydrazine hydrate; dicyclohexyl-carbodiimide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2009.05.085

Reference yield:

: 35418-07-6
methyl 3-(4-aminophenyl)propionate

: 1192365-92-6
3,4-dichloro-N'-(3-(4-(methylsulfonamido)phenyl)propanoyl)benzohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 0 - 20 °C

2: hydrazine hydrate / methanol / 12 h / Reflux

3: dicyclohexyl-carbodiimide / dichloromethane; N,N-dimethyl-formamide / 12 h / 20 °C

With pyridine; hydrazine hydrate; dicyclohexyl-carbodiimide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2009.05.085