Technology Process of benzyl 2,4,6-trideoxy-3-O-methyl-4-C-methoxymethylene-α-L-threo-hexopyranoside
There total 3 articles about benzyl 2,4,6-trideoxy-3-O-methyl-4-C-methoxymethylene-α-L-threo-hexopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) 20 percent NaOH, 2.) 1 percent hydrochloric acid, 3.) molecular sieves 3 Angstroem, 4.) pyridinium chlorochromate
2: 1.) diisopropylamide, 3.) potassium hydride / 1.) THF, 0 deg C, 2.) THF, -78 deg C -> room temperature, 3.) N,N'-dimethylformamide, 1 h
With
hydrogenchloride; sodium hydroxide; 3 A molecular sieve; potassium hydride; diisopropylamine; pyridinium chlorochromate;
DOI:10.1016/S0040-4020(01)87245-8
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) 20 percent NaOH, 2.) 1 percent hydrochloric acid, 3.) molecular sieves 3 Angstroem, 4.) pyridinium chlorochromate
2: 1.) diisopropylamide, 3.) potassium hydride / 1.) THF, 0 deg C, 2.) THF, -78 deg C -> room temperature, 3.) N,N'-dimethylformamide, 1 h
With
hydrogenchloride; sodium hydroxide; 3 A molecular sieve; potassium hydride; diisopropylamine; pyridinium chlorochromate;
DOI:10.1016/S0040-4020(01)87245-8
- Guidance literature:
-
With
potassium hydride; diisopropylamine;
Yield given. Multistep reaction;
1.) THF, 0 deg C, 2.) THF, -78 deg C -> room temperature, 3.) N,N'-dimethylformamide, 1 h;
DOI:10.1016/S0040-4020(01)87245-8
