C₂₄H₂₆INO₆

Base Information

Chemical Name:C₂₄H₂₆INO₆
CAS No.:1032989-92-6
Molecular Formula:C₂₄H₂₆INO₆
Molecular Weight:551.378
Hs Code.:

C<sub>24</sub>H<sub>26</sub>INO<sub>6</sub>

Synonyms:C₂₄H₂₆INO₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₂₆INO₆

Chemical Property:

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Technology Process of C₂₄H₂₆INO₆

There total 5 articles about C₂₄H₂₆INO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 118949-49-8,139462-27-4
4-benzyl-3-[2-(4-methoxy-benzyloxy)-acetyl]-oxazolidin-2-one

: 1032989-91-5
(E)-3-Iodo-but-2-enal

: 1032989-92-6
C₂₄H₂₆INO₆

Guidance literature:: 4-benzyl-3-[2-(4-methoxy-benzyloxy)-acetyl]-oxazolidin-2-one; With di-n-butylboryl trifluoromethanesulfonate; triethylamine; In toluene; at -50 ℃; for 1.5h; Inert atmosphere;

(E)-3-Iodo-but-2-enal; In toluene; at -50 - -30 ℃; for 1.5h; optical yield given as %de; Inert atmosphere;
DOI:10.1039/c2ob25100k

Reference yield:

: 118949-49-8,139462-27-4
4-benzyl-3-[2-(4-methoxy-benzyloxy)-acetyl]-oxazolidin-2-one

: 1032989-91-5
(E)-3-Iodo-but-2-enal

: C₂₄H₂₆INO₆

: 1032989-92-6
C₂₄H₂₆INO₆

Guidance literature:: 4-benzyl-3-[2-(4-methoxy-benzyloxy)-acetyl]-oxazolidin-2-one; With di-n-butylboryl trifluoromethanesulfonate; triethylamine; In toluene; at -50 ℃;

(E)-3-Iodo-but-2-enal; In toluene; at -50 - -30 ℃; Further stages.;
DOI:10.1002/anie.200705565

Reference yield:

: 40217-17-2,90719-32-7,120574-96-1,102029-44-7
(R)-4-(phenylmethyl)-2-oxazolidinone

: 1032989-92-6
C₂₄H₂₆INO₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / -78 - 0 °C / Inert atmosphere

2.1: 20% palladium hydroxide on charcoal; hydrogen / ethyl acetate / 2 h / Inert atmosphere

3.1: trityl tetrafluoroborate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

4.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / toluene / 1.5 h / -50 °C / Inert atmosphere

4.2: 1.5 h / -50 - -30 °C / Inert atmosphere

With n-butyllithium; di-n-butylboryl trifluoromethanesulfonate; 20% palladium hydroxide on charcoal; hydrogen; trityl tetrafluoroborate; triethylamine; In tetrahydrofuran; hexane; ethyl acetate; toluene; 4.1: Evans aldol coupling / 4.2: Evans aldol coupling;
DOI:10.1039/c2ob25100k