(2S,3R)-3-(4-bromophenyl)-3-(diphenylphosphorylamino)-N,N,2-trimethylpropanethioamide

Base Information

Chemical Name:(2S,3R)-3-(4-bromophenyl)-3-(diphenylphosphorylamino)-N,N,2-trimethylpropanethioamide
CAS No.:1182707-49-8
Molecular Formula:C₂₄H₂₆BrN₂OPS
Molecular Weight:501.427
Hs Code.:

Synonyms:(2S,3R)-3-(4-bromophenyl)-3-(diphenylphosphorylamino)-N,N,2-trimethylpropanethioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-3-(4-bromophenyl)-3-(diphenylphosphorylamino)-N,N,2-trimethylpropanethioamide

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Technology Process of (2S,3R)-3-(4-bromophenyl)-3-(diphenylphosphorylamino)-N,N,2-trimethylpropanethioamide

There total 1 articles about (2S,3R)-3-(4-bromophenyl)-3-(diphenylphosphorylamino)-N,N,2-trimethylpropanethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5309-94-4
N,N-Dimethyl-thiopropionamide

: N-(p-bromobenzylidene)diphenylphosphinamide

: 1182707-49-8
(2S,3R)-3-(4-bromophenyl)-3-(diphenylphosphorylamino)-N,N,2-trimethylpropanethioamide

: (2R,3S)-3-(4-bromophenyl)-3-(diphenylphosphorylamino)-N,N,2-trimethylpropanethioamide

: (2S,3R)-3-(4-bromophenyl)-3-(diphenylphosphorylamino)-N,N,2-trimethylpropanethioamide

Guidance literature:: N-(p-bromobenzylidene)diphenylphosphinamide; With tetrakis(actonitrile)copper(I) hexafluorophosphate; (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; In tetrahydrofuran; toluene; at 20 ℃; Inert atmosphere;

N,N-Dimethyl-thiopropionamide; With lithium o-methoxyphenoxide; In tetrahydrofuran; toluene; at 0 ℃; for 42h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.200901588