2-(1',2',3',4',5'-penta-O-acetyl-D-gluco-pentitol-1-yl)-3-methyl-5-phenyl-1,3-thiazolium-4-olate

Base Information

Chemical Name:2-(1',2',3',4',5'-penta-O-acetyl-D-gluco-pentitol-1-yl)-3-methyl-5-phenyl-1,3-thiazolium-4-olate
CAS No.:444716-98-7
Molecular Formula:C₂₅H₂₉NO₁₁S
Molecular Weight:551.571
Hs Code.:

Synonyms:2-(1',2',3',4',5'-penta-O-acetyl-D-gluco-pentitol-1-yl)-3-methyl-5-phenyl-1,3-thiazolium-4-olate

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Chemical Property of 2-(1',2',3',4',5'-penta-O-acetyl-D-gluco-pentitol-1-yl)-3-methyl-5-phenyl-1,3-thiazolium-4-olate

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Technology Process of 2-(1',2',3',4',5'-penta-O-acetyl-D-gluco-pentitol-1-yl)-3-methyl-5-phenyl-1,3-thiazolium-4-olate

There total 2 articles about 2-(1',2',3',4',5'-penta-O-acetyl-D-gluco-pentitol-1-yl)-3-methyl-5-phenyl-1,3-thiazolium-4-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 2912-62-1
α-chlorophenylacetyl chloride

: 289678-02-0
2,3,4,5,6-penta-O-acetyl-N-methyl-D-thiogluconamide

: 444716-98-7
2-(1',2',3',4',5'-penta-O-acetyl-D-gluco-pentitol-1-yl)-3-methyl-5-phenyl-1,3-thiazolium-4-olate

Guidance literature:: In chloroform; for 0.5h; Heating;
DOI:10.1016/j.tet.2006.04.093

Reference yield:

: 147964-50-9
2,3,4,5,6-penta-O-acetyl-N-methyl-D-gluconamide

: 444716-98-7
2-(1',2',3',4',5'-penta-O-acetyl-D-gluco-pentitol-1-yl)-3-methyl-5-phenyl-1,3-thiazolium-4-olate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Lawesson's reagent / benzene

2.1: CHCl₃

2.2: triethylamine / CHCl₃ / 0.5 h / Heating

With Lawessons reagent; In chloroform; benzene;
DOI:10.1016/S0957-4166(02)00104-0

Reference yield: 53.0%

: 78-94-4,25038-87-3
methyl vinyl ketone

: 444716-98-7
2-(1',2',3',4',5'-penta-O-acetyl-D-gluco-pentitol-1-yl)-3-methyl-5-phenyl-1,3-thiazolium-4-olate

: 4-acetyl-6-(1',2',3',4',5'-penta-O-acetyl-D-gluco-pentitol-1-yl)-1-methyl-3-phenylpyrid-2-one

Guidance literature:: methyl vinyl ketone; 2-(1',2',3',4',5'-penta-O-acetyl-D-gluco-pentitol-1-yl)-3-methyl-5-phenyl-1,3-thiazolium-4-olate; In chloroform; for 12h; Heating;

With mercury(II) diacetate; acetic acid; at 20 ℃;
DOI:10.1016/j.tet.2006.04.093