cupreine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

Base Information

Chemical Name:cupreine 9-O-(4-(perfluoro-n-octyl)benzyl) ether
CAS No.:1265815-60-8
Molecular Formula:C₃₄H₂₇F₁₇N₂O₂
Molecular Weight:818.573
Hs Code.:

Synonyms:cupreine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

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Chemical Property of cupreine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

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Technology Process of cupreine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

There total 4 articles about cupreine 9-O-(4-(perfluoro-n-octyl)benzyl) ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1265816-33-8
6'-(methoxymethyl)cupreine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

: 1265815-60-8
cupreine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

Guidance literature:: With hydrogenchloride; water; In methanol; at 50 ℃; for 0.666667h; Inert atmosphere;
DOI:10.1039/c0gc00619j

Reference yield:

: 1265816-31-6
6'-(methoxymethyl)cupreine

: 1265815-60-8
cupreine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 °C / Inert atmosphere

1.2: 2 h / 20 °C / Inert atmosphere

2.1: hydrogenchloride; water / methanol / 0.67 h / 50 °C / Inert atmosphere

With hydrogenchloride; water; sodium hydride; In methanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c0gc00619j

Reference yield:

: 524-63-0,70877-75-7
(3ξ,8α,9R)-cinchonan-6',9-diol

: 1265815-60-8
cupreine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 °C / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

3.1: hydrogenchloride; water / methanol / 0.67 h / 50 °C / Inert atmosphere

With hydrogenchloride; water; sodium hydride; In methanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c0gc00619j