methyl 9-(3'R,5'R-dibenzoyloxy-6'S-methyl-(2H)-tetrahydropyran-2'-yloxy)nonanoate

Base Information

Chemical Name:methyl 9-(3'R,5'R-dibenzoyloxy-6'S-methyl-(2H)-tetrahydropyran-2'-yloxy)nonanoate
CAS No.:1355683-76-9
Molecular Formula:C₃₀H₃₈O₈
Molecular Weight:526.627
Hs Code.:

Synonyms:methyl 9-(3'R,5'R-dibenzoyloxy-6'S-methyl-(2H)-tetrahydropyran-2'-yloxy)nonanoate

Suppliers and Price of methyl 9-(3'R,5'R-dibenzoyloxy-6'S-methyl-(2H)-tetrahydropyran-2'-yloxy)nonanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of methyl 9-(3'R,5'R-dibenzoyloxy-6'S-methyl-(2H)-tetrahydropyran-2'-yloxy)nonanoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of methyl 9-(3'R,5'R-dibenzoyloxy-6'S-methyl-(2H)-tetrahydropyran-2'-yloxy)nonanoate

There total 2 articles about methyl 9-(3'R,5'R-dibenzoyloxy-6'S-methyl-(2H)-tetrahydropyran-2'-yloxy)nonanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 34957-73-8
methyl 9-hydroxynonanoate

: 168170-58-9
(3’R,5’R-dibenzoyloxy-6’S-methyl-(2H)-tetrahydropyran-2-yloxy)-1-(2,2,2-trichloroacetimide)

: 1355683-76-9
methyl 9-(3'R,5'R-dibenzoyloxy-6'S-methyl-(2H)-tetrahydropyran-2'-yloxy)nonanoate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1021/ja210202y

Reference yield:

: 2104-19-0
azelaic monomethyl ester

: 1355683-76-9
methyl 9-(3'R,5'R-dibenzoyloxy-6'S-methyl-(2H)-tetrahydropyran-2'-yloxy)nonanoate

Guidance literature:: Multi-step reaction with 2 steps

1: borane-THF / tetrahydrofuran / 4 h / -20 - 20 °C

2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / 0 °C

With borane-THF; trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane;