tetrakis(mesitylsulfonyl)-N,N'-bis(4-piperidinylmethyl)-1,4-diaminobutane

Base Information

Chemical Name:tetrakis(mesitylsulfonyl)-N,N'-bis(4-piperidinylmethyl)-1,4-diaminobutane
CAS No.:165288-18-6
Molecular Formula:C₅₂H₇₄N₄O₈S₄
Molecular Weight:1011.45
Hs Code.:

Synonyms:tetrakis(mesitylsulfonyl)-N,N'-bis(4-piperidinylmethyl)-1,4-diaminobutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetrakis(mesitylsulfonyl)-N,N'-bis(4-piperidinylmethyl)-1,4-diaminobutane

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Technology Process of tetrakis(mesitylsulfonyl)-N,N'-bis(4-piperidinylmethyl)-1,4-diaminobutane

There total 3 articles about tetrakis(mesitylsulfonyl)-N,N'-bis(4-piperidinylmethyl)-1,4-diaminobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 110-52-1
1,4-dibromo-butane

: 165288-17-5
N,N'-bis(mesitylsulfonyl)-4-(aminomethyl)piperidine

: 165288-18-6
tetrakis(mesitylsulfonyl)-N,N'-bis(4-piperidinylmethyl)-1,4-diaminobutane

Guidance literature:: N,N'-bis(mesitylsulfonyl)-4-(aminomethyl)piperidine; With sodium hydride; sodium iodide; In DMF (N,N-dimethyl-formamide); at 0 - 20 ℃; for 1.75h;

1,4-dibromo-butane; In DMF (N,N-dimethyl-formamide); at 20 - 84 ℃; for 19h;

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 165288-18-6
tetrakis(mesitylsulfonyl)-N,N'-bis(4-piperidinylmethyl)-1,4-diaminobutane

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / 1N aq. NaOH / CH₂Cl₂ / 24 h / 0 - 20 °C

2: 1.) NaH, NaI / 1.) DMF, RT, 105 min, 2.) DMF, 84 deg C, 19 h

With sodium hydroxide; sodium hydride; sodium iodide; In dichloromethane;
DOI:10.1021/jm00013a003

Reference yield:

: 7144-05-0
4-Aminomethylpiperidine

: 165288-18-6
tetrakis(mesitylsulfonyl)-N,N'-bis(4-piperidinylmethyl)-1,4-diaminobutane

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / 1N aq. NaOH / CH₂Cl₂ / 24 h / 0 - 20 °C

2: 1.) NaH, NaI / 1.) DMF, RT, 105 min, 2.) DMF, 84 deg C, 19 h

With sodium hydroxide; sodium hydride; sodium iodide; In dichloromethane;
DOI:10.1021/jm00013a003