methyl 6-deoxy-2,3,4-tri-O-acetyl-6-N-(5R)-phenyl-azepan-2-one-α-D-mannopyranoside.

Base Information

Chemical Name:methyl 6-deoxy-2,3,4-tri-O-acetyl-6-N-(5R)-phenyl-azepan-2-one-α-D-mannopyranoside.
CAS No.:1270918-36-9
Molecular Formula:C₂₅H₃₃NO₉
Molecular Weight:491.538
Hs Code.:

Synonyms:methyl 6-deoxy-2,3,4-tri-O-acetyl-6-N-(5R)-phenyl-azepan-2-one-α-D-mannopyranoside.

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 6-deoxy-2,3,4-tri-O-acetyl-6-N-(5R)-phenyl-azepan-2-one-α-D-mannopyranoside.

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Technology Process of methyl 6-deoxy-2,3,4-tri-O-acetyl-6-N-(5R)-phenyl-azepan-2-one-α-D-mannopyranoside.

There total 2 articles about methyl 6-deoxy-2,3,4-tri-O-acetyl-6-N-(5R)-phenyl-azepan-2-one-α-D-mannopyranoside. which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1270918-35-8
methyl 6-deoxy-6-N-(5R)-phenyl-azepan-2-one-α-D-mannopyranoside

: 108-24-7
acetic anhydride

: 1270918-36-9
methyl 6-deoxy-2,3,4-tri-O-acetyl-6-N-(5R)-phenyl-azepan-2-one-α-D-mannopyranoside.

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1039/c0ob00719f

Reference yield:

: 66224-56-4
methyl 6-azido-6-deoxy-α-D-mannopyranoside

: 4894-75-1
1-phenyl-4-cyclohexanone

: 1270918-36-9
methyl 6-deoxy-2,3,4-tri-O-acetyl-6-N-(5R)-phenyl-azepan-2-one-α-D-mannopyranoside.

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere

1.2: 1 h / Inert atmosphere

2.1: pyridine; dmap / dichloromethane / 16 h / 20 °C / Inert atmosphere

With pyridine; dmap; boron trifluoride diethyl etherate; In dichloromethane; 1.1: Aube reaction / 1.2: Aube reaction;
DOI:10.1039/c0ob00719f