(benzyloxy)germanium(IV) α,β,γ-triazatetrabenzcorrole hemihydrate

Base Information

Chemical Name:(benzyloxy)germanium(IV) α,β,γ-triazatetrabenzcorrole hemihydrate
CAS No.:100228-58-8
Molecular Formula:C₃₉H₂₃GeN₇O*0H₂O
Molecular Weight:687.256
Hs Code.:

Synonyms:(benzyloxy)germanium(IV) α,β,γ-triazatetrabenzcorrole hemihydrate

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Chemical Property of (benzyloxy)germanium(IV) α,β,γ-triazatetrabenzcorrole hemihydrate

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Technology Process of (benzyloxy)germanium(IV) α,β,γ-triazatetrabenzcorrole hemihydrate

There total 1 articles about (benzyloxy)germanium(IV) α,β,γ-triazatetrabenzcorrole hemihydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 19566-97-3
dichlorogermanium (IV) phthalocyanine

: 100-51-6,185532-71-2
benzyl alcohol

: 100228-58-8
(benzyloxy)germanium(IV) α,β,γ-triazatetrabenzcorrole hemihydrate

Guidance literature:: With sodium tetrahydroborate; In benzyl alcohol; a mixt. of complex and NaBH4 in benzyl alcohol and anisole was stirred at 160°C for 2 h under Ar atm.; the hot mixt. was filtered under reduced pressure, evapd., washed with ether, the solid was extd. with hot xylene, evapd. at 70°C under reduced pressure, washed with ether and dried in vac. for 1 d at 100°C; elem. anal.;
DOI:10.1021/ja00267a024