2-(4-benzyl-1-piperazinyl)-4-chloro-5,6-trimethylenepyrimidine

Base Information

Chemical Name:2-(4-benzyl-1-piperazinyl)-4-chloro-5,6-trimethylenepyrimidine
CAS No.:78043-15-9
Molecular Formula:C₁₈H₂₁ClN₄
Molecular Weight:328.845
Hs Code.:

Synonyms:2-(4-benzyl-1-piperazinyl)-4-chloro-5,6-trimethylenepyrimidine

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Chemical Property of 2-(4-benzyl-1-piperazinyl)-4-chloro-5,6-trimethylenepyrimidine

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Technology Process of 2-(4-benzyl-1-piperazinyl)-4-chloro-5,6-trimethylenepyrimidine

There total 5 articles about 2-(4-benzyl-1-piperazinyl)-4-chloro-5,6-trimethylenepyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 79051-07-3
2-(4-benzyl-1-piperazinyl)-5,6-trimethylene-4(3H)-pyrimidinone

: 78043-15-9
2-(4-benzyl-1-piperazinyl)-4-chloro-5,6-trimethylenepyrimidine

Guidance literature:: With trichlorophosphate; for 1h; Heating;

Reference yield:

: 120-92-3
cyclopentanone

: 78043-15-9
2-(4-benzyl-1-piperazinyl)-4-chloro-5,6-trimethylenepyrimidine

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / DBU / 7 h / 150 °C / in a sealed tube

2: 39 percent / NaNO₂, AcOH / H₂O / 1.) r.t., 1 h; 2.) reflux, 2 h

3: 70 percent / 3-methyl-butan-1-ol / 3 h / Heating

4: 80 percent / POCl₃ / 1 h / Heating

With acetic acid; sodium nitrite; trichlorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In i-Amyl alcohol; water;

Reference yield:

: 2759-28-6
1-phenylmethylpiperazine

: 78043-15-9
2-(4-benzyl-1-piperazinyl)-4-chloro-5,6-trimethylenepyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / 3-methyl-butan-1-ol / 3 h / Heating

2: 80 percent / POCl₃ / 1 h / Heating

With trichlorophosphate; In i-Amyl alcohol;