C₁₄H₂₀FNO

Base Information

• Chemical Name: C₁₄H₂₀FNO
• CAS No.: 946605-77-2
• Molecular Formula: C₁₄H₂₀FNO
• Molecular Weight: 237.317
• Mol file: 946605-77-2.mol

Synonyms:C₁₄H₂₀FNO

Chemical Property of C₁₄H₂₀FNO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₀FNO

There total 6 articles about C₁₄H₂₀FNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C19H28FNO3 (946605-73-8) → C14H20FNO (946605-77-2)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 3h;

DOI:10.1016/j.bmcl.2007.04.098

Reference yield:

C19H26FNO3 (946605-68-1) → C14H20FNO (946605-77-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / H₂ / Pd/C / 8 h / 20 °C / 2327.23 Torr

2: 100 percent / TFA / CH₂Cl₂ / 3 h / 0 °C

With hydrogen; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane;

DOI:10.1016/j.bmcl.2007.04.098

Reference yield:

C19H28FNO4 (946605-61-4) → C14H20FNO (946605-77-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 50 percent / MsCl; Et₃N / CH₂Cl₂ / 12 h / -78 °C

2: 80 percent / H₂ / Pd/C / 8 h / 20 °C / 2327.23 Torr

3: 100 percent / TFA / CH₂Cl₂ / 3 h / 0 °C

With hydrogen; methanesulfonyl chloride; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane;

DOI:10.1016/j.bmcl.2007.04.098

upstream raw materials:

C₁₉H₂₈FNO₃

2-bromo-4-fluoro-1-isopropoxybenzene

C₁₉H₂₈FNO₄

C₁₉H₂₆FNO₃

Downstream raw materials:

C₂₅H₃₉FN₂O₃

C₂₀H₃₁FN₂O