diphenyl-4b,10a-dihydro-4b,10a benzo<3,4>cyclobuta<1,2-b>benzodioxine-1,4

Base Information

• Chemical Name: diphenyl-4b,10a-dihydro-4b,10a benzo<3,4>cyclobuta<1,2-b>benzodioxine-1,4
• CAS No.: 80232-57-1
• Molecular Formula: C₂₆H₁₈O₂
• Molecular Weight: 362.428

Synonyms:diphenyl-4b,10a-dihydro-4b,10a benzo<3,4>cyclobuta<1,2-b>benzodioxine-1,4

Chemical Property of diphenyl-4b,10a-dihydro-4b,10a benzo<3,4>cyclobuta<1,2-b>benzodioxine-1,4

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

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Technology Process of diphenyl-4b,10a-dihydro-4b,10a benzo<3,4>cyclobuta<1,2-b>benzodioxine-1,4

There total 6 articles about diphenyl-4b,10a-dihydro-4b,10a benzo<3,4>cyclobuta<1,2-b>benzodioxine-1,4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

diphenyl-9,10 diepoxy-4a,10:9,9a tetrahydro-4a,10.9,9a anthracene (80232-59-3) → diphenyl-4b,10a-dihydro-4b,10a benzo<3,4>cyclobuta<1,2-b>benzodioxine-1,4 (80232-57-1)

Guidance literature:

In diethyl ether; for 12h; Ambient temperature;

DOI:10.1016/S0040-4020(01)98961-6

Reference yield: 30.0%

9,10-diphenyl-9,10-dihydro-9,10-epidioxyanthracene (15257-17-7) → 10-phenyl-10-hydroxy-9-anthracenone (5146-30-5) + diphenyl-4b,9b dihydro-4b,9b benzofuro<3,2-b>benzofurane (66927-73-9,80232-58-2) + diphenyl-4b,10a-dihydro-4b,10a benzo<3,4>cyclobuta<1,2-b>benzodioxine-1,4 (80232-57-1) + diphenyl-6,11 dihydro-6,11 epoxy-6,11-dibenzooxepine (36818-38-9)

Guidance literature:

In benzene; for 168h; Further byproducts given; Ambient temperature; Irradiation;

DOI:10.1016/S0040-4020(01)98961-6

Reference yield: 2.0%

N-methylmaleimide (930-88-1) + 9,10-diphenyl-9,10-dihydro-9,10-epidioxyanthracene (15257-17-7) → N-methyl-diphenyl-9,10 diepoxy-4a,10:9,9a ethano-1,4 hexahydro-1,4,4a,10,9,9a anthracenedicarboximide-11,12 (67012-92-4) + diphenyl-4b,9b dihydro-4b,9b benzofuro<3,2-b>benzofurane (66927-73-9,80232-58-2) + diphenyl-4b,10a-dihydro-4b,10a benzo<3,4>cyclobuta<1,2-b>benzodioxine-1,4 (80232-57-1) + diphenyl-6,11 dihydro-6,11 epoxy-6,11-dibenzooxepine (36818-38-9)

Guidance literature:

In diethyl ether; at -37 ℃; for 96h; Further byproducts given; Irradiation;

DOI:10.1016/S0040-4020(01)98961-6

upstream raw materials:

N-methylmaleimide

9,10-diphenyl-9,10-dihydro-9,10-epidioxyanthracene

diphenyl-9,10 diepoxy-4a,10:9,9a tetrahydro-4a,10.9,9a anthracene

9,10-diphenylanthracene

Downstream raw materials:

bromo-7 diphenyl-4b,10a dihydro-4b,10a benzo<3,4>cyclobuta<1,2-b>benzodioxinne-1,4

dibromo-7,8 diphenyl-4b,10a dihydro-4b,10a benzo<3,4>cyclobuta<1,2-b>benzodioxinne-1,4

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