Technology Process of (3S,4S,5S)-4,5-Bis(benzyloxy)-3-methoxyhexanal
There total 5 articles about (3S,4S,5S)-4,5-Bis(benzyloxy)-3-methoxyhexanal which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Celite; sodium acetate; pyridinium chlorochromate;
In
dichloromethane;
for 3h;
DOI:10.1021/jo00168a022
- Guidance literature:
-
Multi-step reaction with 5 steps
2: 2) (EtOH)3N / tetrahydrofuran / Ambient temperature; 1) room temp., 7 d, 2) room temp., 1 h
3: KH / tetrahydrofuran / 1 h
4: 34 percent / 1) 9-BBN, 2) 30percent H2O2 / tetrahydrofuran / 1) 50 degC, 3 d, 2) 1 h
5: 77 percent / pyridinium chlorochromate (PCC), NaOAc, celite / CH2Cl2 / 3 h
With
9-borabicyclo[3.3.1]nonane dimer; triethanolamine; Celite; dihydrogen peroxide; sodium acetate; potassium hydride; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00168a022
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 2) (EtOH)3N / tetrahydrofuran / Ambient temperature; 1) room temp., 7 d, 2) room temp., 1 h
2: KH / tetrahydrofuran / 1 h
3: 34 percent / 1) 9-BBN, 2) 30percent H2O2 / tetrahydrofuran / 1) 50 degC, 3 d, 2) 1 h
4: 77 percent / pyridinium chlorochromate (PCC), NaOAc, celite / CH2Cl2 / 3 h
With
9-borabicyclo[3.3.1]nonane dimer; triethanolamine; Celite; dihydrogen peroxide; sodium acetate; potassium hydride; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00168a022
