2-[2-(1-{4-methoxycarbonyl}phenethyl)-t-butoxycarbonylhydrazine-1-carbonyl]mercaptoethanol

Base Information

Chemical Name:2-[2-(1-{4-methoxycarbonyl}phenethyl)-t-butoxycarbonylhydrazine-1-carbonyl]mercaptoethanol
CAS No.:904290-40-0
Molecular Formula:C₁₈H₂₆N₂O₆S
Molecular Weight:398.48
Hs Code.:

Synonyms:2-[2-(1-{4-methoxycarbonyl}phenethyl)-t-butoxycarbonylhydrazine-1-carbonyl]mercaptoethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[2-(1-{4-methoxycarbonyl}phenethyl)-t-butoxycarbonylhydrazine-1-carbonyl]mercaptoethanol

Chemical Property:

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Technology Process of 2-[2-(1-{4-methoxycarbonyl}phenethyl)-t-butoxycarbonylhydrazine-1-carbonyl]mercaptoethanol

There total 1 articles about 2-[2-(1-{4-methoxycarbonyl}phenethyl)-t-butoxycarbonylhydrazine-1-carbonyl]mercaptoethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 904290-39-7
2-[2-(1-{4-methoxycarbonyl}phenethyl)-t-butoxycarbonylhydrazine-1-carbonyl]mercaptoethyl octanoate

: 904290-40-0
2-[2-(1-{4-methoxycarbonyl}phenethyl)-t-butoxycarbonylhydrazine-1-carbonyl]mercaptoethanol

Guidance literature:: 2-[2-(1-{4-methoxycarbonyl}phenethyl)-t-butoxycarbonylhydrazine-1-carbonyl]mercaptoethyl octanoate; With methanol; sodium methylate; at 0 ℃; for 4h;

With hydrogenchloride; water; In methanol;

Reference yield:

: 904290-40-0
2-[2-(1-{4-methoxycarbonyl}phenethyl)-t-butoxycarbonylhydrazine-1-carbonyl]mercaptoethanol

: 98-59-9
p-toluenesulfonyl chloride

: 904290-41-1
t-butyl 3-[4-(4-methoxycarbonyl)phenethyl]-2-oxo-2H-1,3,4-thiadiazine-4-carboxylate

Guidance literature:: 2-[2-(1-{4-methoxycarbonyl}phenethyl)-t-butoxycarbonylhydrazine-1-carbonyl]mercaptoethanol; p-toluenesulfonyl chloride; With triethylamine; In dichloromethane; at 20 ℃; for 18h;

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 3h;