5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene-1,2,10,11-tetraone

Base Information

• Chemical Name: 5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene-1,2,10,11-tetraone
• CAS No.: 1374751-50-4
• Molecular Formula: C₇₈H₅₄O₄
• Molecular Weight: 1055.28

Synonyms:5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene-1,2,10,11-tetraone

Chemical Property of 5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene-1,2,10,11-tetraone

Chemical Property:

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Technology Process of 5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene-1,2,10,11-tetraone

There total 1 articles about 5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene-1,2,10,11-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene-2,11-diol (1374751-49-1) → 5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene-1,2,10,11-tetraone (1374751-50-4)

Guidance literature:

With bis-[(trifluoroacetoxy)iodo]benzene; In water; N,N-dimethyl-formamide; at 20 ℃; for 3h; Inert atmosphere; Darkness;

DOI:10.1021/ol300743f

Reference yield: 79.0%

5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene-1,2,10,11-tetraone (1374751-50-4) → 5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene-1,2,10,11-tetraol (1374751-51-5)

Guidance literature:

With sodium tetrahydroborate; In ethanol; dichloromethane; at 20 ℃; for 4h; Inert atmosphere; Darkness;

DOI:10.1021/ol300743f

Reference yield: 70.0%

5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene-1,2,10,11-tetraone (1374751-50-4) → 3,10-dibromo-5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene-1,2,11,12-tetraol

Guidance literature:

With hydrogen bromide; In dichloromethane; water; at 20 ℃; for 12h; Inert atmosphere; Darkness;

DOI:10.1246/cl.140577

upstream raw materials:

5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene-2,11-diol

Downstream raw materials:

5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene-1,2,10,11-tetraol

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