5-[(benzyloxy)methyl]-5-[(4-methoxyphenoxy)methyl]-3,3-bis(3-methyl-2-butenyl)dihydro-2(3H)-furanone

Base Information

• Chemical Name: 5-[(benzyloxy)methyl]-5-[(4-methoxyphenoxy)methyl]-3,3-bis(3-methyl-2-butenyl)dihydro-2(3H)-furanone
• CAS No.: 881850-38-0
• Molecular Formula: C₃₀H₃₈O₅
• Molecular Weight: 478.629

Synonyms:5-[(benzyloxy)methyl]-5-[(4-methoxyphenoxy)methyl]-3,3-bis(3-methyl-2-butenyl)dihydro-2(3H)-furanone

Chemical Property of 5-[(benzyloxy)methyl]-5-[(4-methoxyphenoxy)methyl]-3,3-bis(3-methyl-2-butenyl)dihydro-2(3H)-furanone

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Technology Process of 5-[(benzyloxy)methyl]-5-[(4-methoxyphenoxy)methyl]-3,3-bis(3-methyl-2-butenyl)dihydro-2(3H)-furanone

There total 1 articles about 5-[(benzyloxy)methyl]-5-[(4-methoxyphenoxy)methyl]-3,3-bis(3-methyl-2-butenyl)dihydro-2(3H)-furanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

prenyl bromide (870-63-3) + 5-[(4-methoxyphenoxy)methyl]-5-[(phenylmethoxy)methyl]-3,4,5-trihydrofuran-2-one (213828-30-9) → 5-[(benzyloxy)methyl]-5-[(4-methoxyphenoxy)methyl]-3,3-bis(3-methyl-2-butenyl)dihydro-2(3H)-furanone (881850-38-0)

Guidance literature:

5-[(4-methoxyphenoxy)methyl]-5-[(phenylmethoxy)methyl]-3,4,5-trihydrofuran-2-one; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h;

prenyl bromide; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; at -78 ℃; for 1h;

DOI:10.1021/jm0509391

Reference yield:

5-[(benzyloxy)methyl]-5-[(4-methoxyphenoxy)methyl]-3,3-bis(3-methyl-2-butenyl)dihydro-2(3H)-furanone (881850-38-0) → 5-hydroxymethyl-5-(4-methoxy-phenoxymethyl)-3,3-bis-(3-methyl-but-2-enyl)-dihydro-furan-2-one

Guidance literature:

With boron trichloride; In dichloromethane; at -78 ℃; for 2h;

DOI:10.1021/jm0509391

Reference yield:

5-[(benzyloxy)methyl]-5-[(4-methoxyphenoxy)methyl]-3,3-bis(3-methyl-2-butenyl)dihydro-2(3H)-furanone (881850-38-0) → 5-hydroxymethyl-5-(4-methoxy-phenoxymethyl)-3,3-bis-(3-methyl-butyl)-dihydro-furan-2-one

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol;

DOI:10.1021/jm0509391

upstream raw materials:

prenyl bromide

5-[(4-methoxyphenoxy)methyl]-5-[(phenylmethoxy)methyl]-3,4,5-trihydrofuran-2-one

Downstream raw materials:

2,2-dimethyl-propionic acid 2-(4-methoxy-phenoxymethyl)-4,4-bis-(3-methyl-butyl)-5-oxo-tetrahydro-furan-2-ylmethyl ester

2,2-dimethyl-propionic acid 2-(4-methoxy-phenoxymethyl)-4,4-bis-(3-methyl-but-2-enyl)-5-oxo-tetrahydro-furan-2-ylmethyl ester

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