1,2,3,4,4a,12a-hexahydro-11H,12H-4a-hydroxy-11-methyl-12-phenylbenzopyrano<3,2-c><1,2>benzothiazine 10,10-dioxide

Base Information

Chemical Name:1,2,3,4,4a,12a-hexahydro-11H,12H-4a-hydroxy-11-methyl-12-phenylbenzopyrano<3,2-c><1,2>benzothiazine 10,10-dioxide
CAS No.:131769-19-2
Molecular Formula:C₂₂H₂₃NO₄S
Molecular Weight:397.495
Hs Code.:

Synonyms:1,2,3,4,4a,12a-hexahydro-11H,12H-4a-hydroxy-11-methyl-12-phenylbenzopyrano<3,2-c><1,2>benzothiazine 10,10-dioxide

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Chemical Property of 1,2,3,4,4a,12a-hexahydro-11H,12H-4a-hydroxy-11-methyl-12-phenylbenzopyrano<3,2-c><1,2>benzothiazine 10,10-dioxide

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Technology Process of 1,2,3,4,4a,12a-hexahydro-11H,12H-4a-hydroxy-11-methyl-12-phenylbenzopyrano<3,2-c><1,2>benzothiazine 10,10-dioxide

There total 4 articles about 1,2,3,4,4a,12a-hexahydro-11H,12H-4a-hydroxy-11-methyl-12-phenylbenzopyrano<3,2-c><1,2>benzothiazine 10,10-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: (7R,7aS,11aR)-6-Methyl-11a-morpholin-4-yl-7-phenyl-7a,8,9,10,11,11a-hexahydro-6H,7H-12-oxa-5-thia-6-aza-benzo[a]anthracene 5,5-dioxide

: 131769-19-2
1,2,3,4,4a,12a-hexahydro-11H,12H-4a-hydroxy-11-methyl-12-phenylbenzopyrano<3,2-c><1,2>benzothiazine 10,10-dioxide

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; for 12h; Ambient temperature;

Reference yield: 85.0%

: (7R,7aR,11aR)-6-Methyl-11a-morpholin-4-yl-7-phenyl-7a,8,9,10,11,11a-hexahydro-6H,7H-12-oxa-5-thia-6-aza-benzo[a]anthracene 5,5-dioxide

: 131769-19-2
1,2,3,4,4a,12a-hexahydro-11H,12H-4a-hydroxy-11-methyl-12-phenylbenzopyrano<3,2-c><1,2>benzothiazine 10,10-dioxide

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; for 12h; Ambient temperature;

Reference yield:

: 670-80-4
4-cyclohexen-1-ylmorpholine

: 131769-19-2
1,2,3,4,4a,12a-hexahydro-11H,12H-4a-hydroxy-11-methyl-12-phenylbenzopyrano<3,2-c><1,2>benzothiazine 10,10-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / toluene / 80 °C

2: 85 percent / 0.1 N hydrochloric acid / dioxane / 12 h / Ambient temperature

With hydrogenchloride; In 1,4-dioxane; toluene;