C₁₂H₁₄BrN₃O₂

Base Information

Chemical Name:C₁₂H₁₄BrN₃O₂
CAS No.:1608506-61-1
Molecular Formula:C₁₂H₁₄BrN₃O₂
Molecular Weight:312.166
Hs Code.:

C<sub>12</sub>H<sub>14</sub>BrN<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₂H₁₄BrN₃O₂

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Chemical Property of C₁₂H₁₄BrN₃O₂

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Technology Process of C₁₂H₁₄BrN₃O₂

There total 6 articles about C₁₂H₁₄BrN₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1608506-51-9
C₁₂H₁₃BrN₄

: 1608506-61-1
C₁₂H₁₄BrN₃O₂

Guidance literature:: With water; sodium hydroxide; In ethanol; at 85 ℃; for 10h; Inert atmosphere;
DOI:10.1021/ol501058a

Reference yield:

: 107558-73-6
diethyl 2-(3-bromobenzyl)-malonate

: 1608506-61-1
C₁₂H₁₄BrN₃O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / mineral oil; dimethyl sulfoxide; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

1.2: 60 h / Inert atmosphere

2.1: lithium chloride / dimethyl sulfoxide / 4 h / 140 °C / Inert atmosphere

3.1: lithium chloride; potassium borohydride / tetrahydrofuran / 24 h / Inert atmosphere; Reflux

4.1: triethylamine; dmap / dichloromethane / 24 h / 20 °C / Inert atmosphere

5.1: sodium azide; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 12 h / 40 °C / Inert atmosphere

6.1: sodium hydroxide; water / ethanol / 10 h / 85 °C / Inert atmosphere

With dmap; sodium azide; potassium borohydride; water; tetra-(n-butyl)ammonium iodide; sodium hydride; triethylamine; lithium chloride; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol501058a

Reference yield:

: 1608506-23-5
C₁₄H₁₆BrNO₂

: 1608506-61-1
C₁₂H₁₄BrN₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1: lithium chloride; potassium borohydride / tetrahydrofuran / 24 h / Inert atmosphere; Reflux

2: triethylamine; dmap / dichloromethane / 24 h / 20 °C / Inert atmosphere

3: sodium azide; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 12 h / 40 °C / Inert atmosphere

4: sodium hydroxide; water / ethanol / 10 h / 85 °C / Inert atmosphere

With dmap; sodium azide; potassium borohydride; water; tetra-(n-butyl)ammonium iodide; triethylamine; lithium chloride; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol501058a