Technology Process of C33H38Cl2N6O2
There total 7 articles about C33H38Cl2N6O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
diethyl cyanophosphonate; triethylamine;
In
dichloromethane;
at 20 ℃;
for 69h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetonitrile / water bath
1.2: 0.25 h
2.1: hydrogenchloride / diethyl ether; dichloromethane; acetonitrile / 1 h
2.2: 21 h / 0 - 20 °C
3.1: triethylamine / dichloromethane / 18 h / 20 °C
4.1: sodium hydroxide; water / 1,4-dioxane; methanol / 144 h / 20 °C
4.2: 18 h
5.1: diethyl cyanophosphonate; triethylamine / dichloromethane / 69 h / 20 °C
With
hydrogenchloride; sodium hydroxide; diethyl cyanophosphonate; water; triethylamine;
In
1,4-dioxane; methanol; diethyl ether; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride / diethyl ether; dichloromethane; acetonitrile / 1 h
1.2: 21 h / 0 - 20 °C
2.1: triethylamine / dichloromethane / 18 h / 20 °C
3.1: sodium hydroxide; water / 1,4-dioxane; methanol / 144 h / 20 °C
3.2: 18 h
4.1: diethyl cyanophosphonate; triethylamine / dichloromethane / 69 h / 20 °C
With
hydrogenchloride; sodium hydroxide; diethyl cyanophosphonate; water; triethylamine;
In
1,4-dioxane; methanol; diethyl ether; dichloromethane; acetonitrile;