methyl 6-<<4-phenyl>sulfonyl>hexanoate

Base Information

Chemical Name:methyl 6-<<4-phenyl>sulfonyl>hexanoate
CAS No.:125174-18-7
Molecular Formula:C₁₇H₂₅Cl₂NO₄S
Molecular Weight:410.362
Hs Code.:

methyl 6-<<4-<N,N-bis(2-chloroethyl)amino>phenyl>sulfonyl>hexanoate

Synonyms:methyl 6-<<4-phenyl>sulfonyl>hexanoate

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Chemical Property of methyl 6-<<4-phenyl>sulfonyl>hexanoate

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Technology Process of methyl 6-<<4-phenyl>sulfonyl>hexanoate

There total 6 articles about methyl 6-<<4-phenyl>sulfonyl>hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 125173-96-8
6-{4-[Bis-(2-chloro-ethyl)-amino]-phenylsulfanyl}-hexanoic acid methyl ester

: 125174-18-7
methyl 6-<<4-phenyl>sulfonyl>hexanoate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 8h;
DOI:10.1021/jm00166a015

Reference yield:

: 14273-90-6
methyl 6-bromohexanoate

: 125174-18-7
methyl 6-<<4-phenyl>sulfonyl>hexanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / methanol / 1.5 h / Heating

2: H₂ / Pd/C / methanol / 17 h

3: 27 percent / AcOH / CH₂Cl₂ / 72 h / 20 °C

4: SOCl₂ / 1,2-dichloro-ethane; dimethylformamide / 0.42 h / Heating

5: 84 percent / 3-chloroperbenzoic acid / CH₂Cl₂ / 8 h / 20 °C

With thionyl chloride; hydrogen; acetic acid; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00166a015

Reference yield:

: 125173-93-5
methyl 6-<(4-nitrophenyl)thio>hexanoate

: 125174-18-7
methyl 6-<<4-phenyl>sulfonyl>hexanoate

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd/C / methanol / 17 h

2: 27 percent / AcOH / CH₂Cl₂ / 72 h / 20 °C

3: SOCl₂ / 1,2-dichloro-ethane; dimethylformamide / 0.42 h / Heating

4: 84 percent / 3-chloroperbenzoic acid / CH₂Cl₂ / 8 h / 20 °C

With thionyl chloride; hydrogen; acetic acid; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00166a015